N₂-(4-(allyloxy)benzyl)-N₄-(3-(allyloxy)phenyl)-6-(2,2,2-trifluoroethoxy)-1,3,5-triazine-2,4-diamine trifluoroacetate

Base Information

• Chemical Name: N₂-(4-(allyloxy)benzyl)-N₄-(3-(allyloxy)phenyl)-6-(2,2,2-trifluoroethoxy)-1,3,5-triazine-2,4-diamine trifluoroacetate
• CAS No.: 1346652-11-6
• Molecular Formula: C₂HF₃O₂*C₂₄H₂₄F₃N₅O₃
• Molecular Weight: 601.505

Synonyms:N₂-(4-(allyloxy)benzyl)-N₄-(3-(allyloxy)phenyl)-6-(2,2,2-trifluoroethoxy)-1,3,5-triazine-2,4-diamine trifluoroacetate

Chemical Property of N₂-(4-(allyloxy)benzyl)-N₄-(3-(allyloxy)phenyl)-6-(2,2,2-trifluoroethoxy)-1,3,5-triazine-2,4-diamine trifluoroacetate

Chemical Property:

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Technology Process of N₂-(4-(allyloxy)benzyl)-N₄-(3-(allyloxy)phenyl)-6-(2,2,2-trifluoroethoxy)-1,3,5-triazine-2,4-diamine trifluoroacetate

There total 4 articles about N₂-(4-(allyloxy)benzyl)-N₄-(3-(allyloxy)phenyl)-6-(2,2,2-trifluoroethoxy)-1,3,5-triazine-2,4-diamine trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.4%

4-((4-(3-(allyloxy)phenylamino)-6-(2,2,2-trifluoroethoxy)-1,3,5-triazin-2-ylamino)-methyl)phenol trifluoroacetate (1346652-09-2) + allyl bromide (106-95-6) → N2-(4-(allyloxy)benzyl)-N4-(3-(allyloxy)phenyl)-6-(2,2,2-trifluoroethoxy)-1,3,5-triazine-2,4-diamine trifluoroacetate (1346652-11-6)

Guidance literature:

4-((4-(3-(allyloxy)phenylamino)-6-(2,2,2-trifluoroethoxy)-1,3,5-triazin-2-ylamino)-methyl)phenol trifluoroacetate; With caesium carbonate; In N,N-dimethyl-formamide; at 45 ℃; for 0.333333h;

allyl bromide; In N,N-dimethyl-formamide; at 20 ℃; for 72h;

Reference yield:

3-allyloxy-phenylamine (74900-81-5) → N2-(4-(allyloxy)benzyl)-N4-(3-(allyloxy)phenyl)-6-(2,2,2-trifluoroethoxy)-1,3,5-triazine-2,4-diamine trifluoroacetate (1346652-11-6)

Guidance literature:

Multi-step reaction with 2 steps

1.1: N-ethyl-N,N-diisopropylamine / 1-Methylpyrrolidine / 0.5 h / 20 °C

1.2: 16 h / 20 °C

2.1: caesium carbonate / N,N-dimethyl-formamide / 0.33 h / 45 °C

2.2: 72 h / 20 °C

With caesium carbonate; N-ethyl-N,N-diisopropylamine; In 1-Methylpyrrolidine; N,N-dimethyl-formamide;

Reference yield:

2,4-dichloro-6-(2,2,2-trifluoroethoxy)-1,3,5-triazine (185677-00-3) → N2-(4-(allyloxy)benzyl)-N4-(3-(allyloxy)phenyl)-6-(2,2,2-trifluoroethoxy)-1,3,5-triazine-2,4-diamine trifluoroacetate (1346652-11-6)

Guidance literature:

Multi-step reaction with 2 steps

1.1: N-ethyl-N,N-diisopropylamine / 1-Methylpyrrolidine / 0.5 h / 20 °C

1.2: 16 h / 20 °C

2.1: caesium carbonate / N,N-dimethyl-formamide / 0.33 h / 45 °C

2.2: 72 h / 20 °C

With caesium carbonate; N-ethyl-N,N-diisopropylamine; In 1-Methylpyrrolidine; N,N-dimethyl-formamide;

upstream raw materials:

4-((4-(3-(allyloxy)phenylamino)-6-(2,2,2-trifluoroethoxy)-1,3,5-triazin-2-ylamino)-methyl)phenol trifluoroacetate

allyl bromide

4-aminomethylphenol

3-allyloxy-phenylamine

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