(2R,3R,4R,5R)-2,5-dibenzoyloxy-3,4-O-(1-methylethylidene)-3,4-hexanediol

Base Information

Chemical Name:(2R,3R,4R,5R)-2,5-dibenzoyloxy-3,4-O-(1-methylethylidene)-3,4-hexanediol
CAS No.:159716-54-8
Molecular Formula:C₂₃H₂₆O₆
Molecular Weight:398.456
Hs Code.:

Synonyms:(2R,3R,4R,5R)-2,5-dibenzoyloxy-3,4-O-(1-methylethylidene)-3,4-hexanediol

Suppliers and Price of (2R,3R,4R,5R)-2,5-dibenzoyloxy-3,4-O-(1-methylethylidene)-3,4-hexanediol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,3R,4R,5R)-2,5-dibenzoyloxy-3,4-O-(1-methylethylidene)-3,4-hexanediol

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Technology Process of (2R,3R,4R,5R)-2,5-dibenzoyloxy-3,4-O-(1-methylethylidene)-3,4-hexanediol

There total 1 articles about (2R,3R,4R,5R)-2,5-dibenzoyloxy-3,4-O-(1-methylethylidene)-3,4-hexanediol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 74044-75-0
(2R,3R,4R,5R)-3,4-O-(1-methylethylidene)-2,3,4,5-hexanetetraol

: 98-88-4
benzoyl chloride

: 159716-54-8
(2R,3R,4R,5R)-2,5-dibenzoyloxy-3,4-O-(1-methylethylidene)-3,4-hexanediol

Guidance literature:: With pyridine; at 0 ℃; for 1h;
DOI:10.1016/S0957-4166(00)86245-X

Reference yield: 74.0%

: 159716-54-8
(2R,3R,4R,5R)-2,5-dibenzoyloxy-3,4-O-(1-methylethylidene)-3,4-hexanediol

: 159716-56-0
C₂₀H₂₂O₆

Guidance literature:: With trifluoroacetic acid; at 0 ℃; for 1h;
DOI:10.1016/S0957-4166(00)86245-X

Reference yield:

: 159716-54-8
(2R,3R,4R,5R)-2,5-dibenzoyloxy-3,4-O-(1-methylethylidene)-3,4-hexanediol

: 159716-58-2
Benzoic acid (E)-(R)-1-methyl-4-oxo-but-2-enyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 74 percent / 90percent aq. TFA / 1 h / 0 °C

2: 87 percent / Pb(OAc)4 / benzene / 1 h / Ambient temperature

3: 72 percent / benzene / 6 h / Heating

With lead(IV) acetate; trifluoroacetic acid; In benzene;
DOI:10.1016/S0957-4166(00)86245-X