C₁₇H₂₁BrO₂

Base Information

Chemical Name:C₁₇H₂₁BrO₂
CAS No.:1426819-12-6
Molecular Formula:C₁₇H₂₁BrO₂
Molecular Weight:337.257
Hs Code.:

C<sub>17</sub>H<sub>21</sub>BrO<sub>2</sub>

Synonyms:C₁₇H₂₁BrO₂

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Chemical Property of C₁₇H₂₁BrO₂

Chemical Property:

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Technology Process of C₁₇H₂₁BrO₂

There total 9 articles about C₁₇H₂₁BrO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₇H₂₃BrO₂

: 1426819-12-6
C₁₇H₂₁BrO₂

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 20 ℃; regioselective reaction;
DOI:10.1016/j.tetlet.2013.01.115

Reference yield:

: 1426819-03-5
C₁₀H₁₅BrO

: 1426819-12-6
C₁₇H₂₁BrO₂

Guidance literature:: Multi-step reaction with 5 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene; dmap / dichloromethane-d2 / 0 - 20 °C

2: K₂OsO₂*2H₂O; potassium hexacyanoferrate(III); 9-O-(9'-Phenanthryl)-dihydroquinine / 20 h / 0 °C

3: camphor-10-sulfonic acid / dichloromethane / Reflux

4: diisobutylaluminium hydride / toluene / 100 °C

5: Dess-Martin periodane / dichloromethane / 20 °C

With dmap; camphor-10-sulfonic acid; K₂OsO₂*2H₂O; diisobutylaluminium hydride; Dess-Martin periodane; 9-O-(9'-Phenanthryl)-dihydroquinine; 1,8-diazabicyclo[5.4.0]undec-7-ene; potassium hexacyanoferrate(III); In dichloromethane; dichloromethane-d2; toluene; 2: |Sharpless Dihydroxylation / 5: |Dess-Martin Oxidation;
DOI:10.1016/j.tetlet.2013.01.115

Reference yield:

: 4773-87-9
3-bromo-2,4-dimethylpenta-1,3-diene

: 1426819-12-6
C₁₇H₂₁BrO₂

Guidance literature:: Multi-step reaction with 8 steps

1: neat (no solvent) / Reflux

2: triethylamine / dichloromethane / 20 °C

3: lithium aluminium tetrahydride / tetrahydrofuran / -40 °C

4: 1,8-diazabicyclo[5.4.0]undec-7-ene; dmap / dichloromethane-d2 / 0 - 20 °C

5: K₂OsO₂*2H₂O; potassium hexacyanoferrate(III); 9-O-(9'-Phenanthryl)-dihydroquinine / 20 h / 0 °C

6: camphor-10-sulfonic acid / dichloromethane / Reflux

7: diisobutylaluminium hydride / toluene / 100 °C

8: Dess-Martin periodane / dichloromethane / 20 °C

With dmap; lithium aluminium tetrahydride; camphor-10-sulfonic acid; K₂OsO₂*2H₂O; diisobutylaluminium hydride; Dess-Martin periodane; 9-O-(9'-Phenanthryl)-dihydroquinine; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; potassium hexacyanoferrate(III); In tetrahydrofuran; dichloromethane; dichloromethane-d2; toluene; 1: |Diels-Alder Cycloaddition / 5: |Sharpless Dihydroxylation / 8: |Dess-Martin Oxidation;
DOI:10.1016/j.tetlet.2013.01.115