tert-butyldimethyl((1S)-1-((4R)-2-phenyl-1,3-dioxolan-4-yl)ethoxy)silane

Base Information

Chemical Name:tert-butyldimethyl((1S)-1-((4R)-2-phenyl-1,3-dioxolan-4-yl)ethoxy)silane
CAS No.:1407163-78-3
Molecular Formula:C₁₇H₂₈O₃Si
Molecular Weight:308.493
Hs Code.:

Synonyms:tert-butyldimethyl((1S)-1-((4R)-2-phenyl-1,3-dioxolan-4-yl)ethoxy)silane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-butyldimethyl((1S)-1-((4R)-2-phenyl-1,3-dioxolan-4-yl)ethoxy)silane

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Technology Process of tert-butyldimethyl((1S)-1-((4R)-2-phenyl-1,3-dioxolan-4-yl)ethoxy)silane

There total 2 articles about tert-butyldimethyl((1S)-1-((4R)-2-phenyl-1,3-dioxolan-4-yl)ethoxy)silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1407163-77-2
(1S)-1-((4R)-2-phenyl-1,3-dioxolan-4-yl)ethanol

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1407163-78-3
tert-butyldimethyl((1S)-1-((4R)-2-phenyl-1,3-dioxolan-4-yl)ethoxy)silane

Guidance literature:: With 1H-imidazole; In dichloromethane; at 0 - 20 ℃; for 2h;
DOI:10.1039/c2ob26396c

Reference yield:

: 1407163-76-1
(1S)-1-((4R)-2-phenyl-1,3-dioxolan-4-yl)ethyl benzoate

: 1407163-78-3
tert-butyldimethyl((1S)-1-((4R)-2-phenyl-1,3-dioxolan-4-yl)ethoxy)silane

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / methanol / 0.5 h / 20 °C

2: 1H-imidazole / dichloromethane / 2 h / 0 - 20 °C

With 1H-imidazole; potassium carbonate; In methanol; dichloromethane;
DOI:10.1039/c2ob26396c

Reference yield: 24.0%

: 1407163-78-3
tert-butyldimethyl((1S)-1-((4R)-2-phenyl-1,3-dioxolan-4-yl)ethoxy)silane

: 1407163-79-4
(2R,3S)-2-(benzyloxy)-3-(tert-butyldimethylsilyloxy)butan-1-ol

: 1407163-83-0
C₁₇H₃₀O₃Si

Guidance literature:: With diisobutylaluminium hydride; In dichloromethane; toluene; at -40 ℃; for 1h; regioselective reaction;
DOI:10.1039/c2ob26396c