N-(2,4-dichlorobenzyl)butan-1-amine

Base Information

• Chemical Name: N-(2,4-dichlorobenzyl)butan-1-amine
• CAS No.: 22704-59-2
• Molecular Formula: C₁₁H₁₅Cl₂N
• Molecular Weight: 232.153
• Mol file: 22704-59-2.mol

Synonyms:Benzylamine,N-butyl-2,4-dichloro- (6CI,8CI)

Chemical Property of N-(2,4-dichlorobenzyl)butan-1-amine

Chemical Property:

• Vapor Pressure: 0.00172mmHg at 25°C
• Boiling Point: 293.5°C at 760 mmHg
• Flash Point: 131.3°C
• PSA: 12.03000
• Density: 1.135g/cm³
• LogP: 4.27400

Purity/Quality:

99% ^*data from raw suppliers

N-[(2,4-Dichlorophenyl)methyl]butan-1-amine 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-(2,4-dichlorobenzyl)butan-1-amine

There total 3 articles about N-(2,4-dichlorobenzyl)butan-1-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,4-dichlorobenzyliminebutane (75692-61-4) → butyl-(2,4-dichloro-benzyl)-amine (22704-59-2)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; for 2h; Heating;

DOI:10.1021/jm00375a005

Reference yield:

2,4-dichlorobenzaldeyhde (874-42-0) → butyl-(2,4-dichloro-benzyl)-amine (22704-59-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 1 h / Ambient temperature

2: LiAlH₄ / diethyl ether / 2 h / Heating

With lithium aluminium tetrahydride; In diethyl ether;

DOI:10.1021/jm00375a005

Reference yield:

→ butyl-(2,4-dichloro-benzyl)-amine (22704-59-2)

Guidance literature:

/BRN= 3257294/;

DOI:10.1021/ja01523a059 DOI:10.1021/ja01619a035

upstream raw materials:

2,4-dichlorobenzyliminebutane

2,4-dichlorobenzaldeyhde

Downstream raw materials:

C₁₂H₁₄Cl₃NO

Refernces