2-(tert-butyl) 1-(4-nitrophenyl) 1-isopropylhydrazine-1,2-dicarboxylate

Base Information

Chemical Name:2-(tert-butyl) 1-(4-nitrophenyl) 1-isopropylhydrazine-1,2-dicarboxylate
CAS No.:162739-75-5
Molecular Formula:C₁₅H₂₁N₃O₆
Molecular Weight:339.348
Hs Code.:

Synonyms:2-(tert-butyl) 1-(4-nitrophenyl) 1-isopropylhydrazine-1,2-dicarboxylate

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Chemical Property of 2-(tert-butyl) 1-(4-nitrophenyl) 1-isopropylhydrazine-1,2-dicarboxylate

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Technology Process of 2-(tert-butyl) 1-(4-nitrophenyl) 1-isopropylhydrazine-1,2-dicarboxylate

There total 3 articles about 2-(tert-butyl) 1-(4-nitrophenyl) 1-isopropylhydrazine-1,2-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 16689-35-3
tert-butyl 2-(isopropyl)hydrazinecarboxylate

: 7693-46-1
4-Nitrophenyl chloroformate

: 162739-75-5
2-(tert-butyl) 1-(4-nitrophenyl) 1-isopropylhydrazine-1,2-dicarboxylate

Guidance literature:: With pyridine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1039/c8nj03635g

Reference yield:

: 16689-34-2
tert-butyl isopropylidenecarbazate

: 162739-75-5
2-(tert-butyl) 1-(4-nitrophenyl) 1-isopropylhydrazine-1,2-dicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium cyanoborohydride; toluene-4-sulfonic acid / tetrahydrofuran / 1 h / 20 °C

2: pyridine / dichloromethane / 0 - 20 °C / Inert atmosphere

With pyridine; sodium cyanoborohydride; toluene-4-sulfonic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1039/c8nj03635g