C₂₈H₄₂O₉

Base Information

Chemical Name:C₂₈H₄₂O₉
CAS No.:1350963-48-2
Molecular Formula:C₂₈H₄₂O₉
Molecular Weight:522.636
Hs Code.:

C<sub>28</sub>H<sub>42</sub>O<sub>9</sub>

Synonyms:C₂₈H₄₂O₉

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Chemical Property of C₂₈H₄₂O₉

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Technology Process of C₂₈H₄₂O₉

There total 7 articles about C₂₈H₄₂O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1350963-47-1
C₂₇H₄₀O₉

: 74-88-4
methyl iodide

: 1350963-48-2
C₂₈H₄₂O₉

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 0 - 25 ℃; for 12h;
DOI:10.1016/j.tetlet.2011.09.139

Reference yield:

: C₂₉H₄₄O₁₄S₂

: 1350963-48-2
C₂₈H₄₂O₉

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium iodide / 1,2-dimethoxyethane

2.1: dimethylsulfide borane complex / tetrahydrofuran / 20 h / 0 °C

2.2: 3 h / 25 °C

3.1: sodium hydride / tetrahydrofuran / 12 h / 0 - 25 °C

With dimethylsulfide borane complex; sodium hydride; sodium iodide; In tetrahydrofuran; 1,2-dimethoxyethane;
DOI:10.1016/j.tetlet.2011.09.139

Reference yield:

: 1350963-44-8
C₃₀H₄₄O₁₀

: 1350963-48-2
C₂₈H₄₂O₉

Guidance literature:: Multi-step reaction with 5 steps

1.1: water; acetic acid / 12 h / 25 °C

2.1: triethylamine / dichloromethane

3.1: sodium iodide / 1,2-dimethoxyethane

4.1: dimethylsulfide borane complex / tetrahydrofuran / 20 h / 0 °C

4.2: 3 h / 25 °C

5.1: sodium hydride / tetrahydrofuran / 12 h / 0 - 25 °C

With dimethylsulfide borane complex; water; sodium hydride; acetic acid; triethylamine; sodium iodide; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane;
DOI:10.1016/j.tetlet.2011.09.139