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C30H49NO5

Base Information
  • Chemical Name:C30H49NO5
  • CAS No.:1403235-37-9
  • Molecular Formula:C30H49NO5
  • Molecular Weight:503.723
  • Hs Code.:
C<sub>30</sub>H<sub>49</sub>NO<sub>5</sub>

Synonyms:C30H49NO5

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Chemical Property of C30H49NO5
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Technology Process of C30H49NO5

There total 10 articles about C30H49NO5 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With dmap; In toluene; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1021/ol302309c
Guidance literature:
Multi-step reaction with 8 steps
1.1: 4-methylmorpholine N-oxide; osmium(VIII) oxide / tert-butyl alcohol; water; tetrahydrofuran / 12 h / Inert atmosphere
1.2: 3 h / 0 - 20 °C / Inert atmosphere
2.1: di-n-butylboryl trifluoromethanesulfonate / dichloromethane / 0.17 h / 0 °C / Inert atmosphere
2.2: 1 h / 0 °C / Inert atmosphere
2.3: 6 h / -78 - 0 °C / Inert atmosphere
3.1: 2,6-dimethylpyridine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere
4.1: sodium tetrahydroborate / water; tetrahydrofuran / 0 - 20 °C / Inert atmosphere
5.1: triethylamine; dmap / dichloromethane / 0 - 20 °C / Inert atmosphere
6.1: copper dichloride; 1-Phenylprop-1-yne / tetrahydrofuran / 24 h / Inert atmosphere; Reflux
7.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C / Inert atmosphere
8.1: dmap / toluene / 3 h / 20 °C / Inert atmosphere
With 2,6-dimethylpyridine; 1-Phenylprop-1-yne; dmap; sodium tetrahydroborate; osmium(VIII) oxide; di-n-butylboryl trifluoromethanesulfonate; tetrabutyl ammonium fluoride; 4-methylmorpholine N-oxide; triethylamine; copper dichloride; In tetrahydrofuran; dichloromethane; water; toluene; tert-butyl alcohol; 2.1: |Evans Aldol Reaction / 2.2: |Evans Aldol Reaction / 2.3: |Evans Aldol Reaction;
DOI:10.1021/ol302309c
Guidance literature:
Multi-step reaction with 7 steps
1.1: di-n-butylboryl trifluoromethanesulfonate / dichloromethane / 0.17 h / 0 °C / Inert atmosphere
1.2: 1 h / 0 °C / Inert atmosphere
1.3: 6 h / -78 - 0 °C / Inert atmosphere
2.1: 2,6-dimethylpyridine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere
3.1: sodium tetrahydroborate / water; tetrahydrofuran / 0 - 20 °C / Inert atmosphere
4.1: triethylamine; dmap / dichloromethane / 0 - 20 °C / Inert atmosphere
5.1: copper dichloride; 1-Phenylprop-1-yne / tetrahydrofuran / 24 h / Inert atmosphere; Reflux
6.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C / Inert atmosphere
7.1: dmap / toluene / 3 h / 20 °C / Inert atmosphere
With 2,6-dimethylpyridine; 1-Phenylprop-1-yne; dmap; sodium tetrahydroborate; di-n-butylboryl trifluoromethanesulfonate; tetrabutyl ammonium fluoride; triethylamine; copper dichloride; In tetrahydrofuran; dichloromethane; water; toluene; 1.1: |Evans Aldol Reaction / 1.2: |Evans Aldol Reaction / 1.3: |Evans Aldol Reaction;
DOI:10.1021/ol302309c
upstream raw materials:

C14H20O

(3S)-5-(benzyloxy)-3-methylpentanal

C26H33NO5

C32H47NO5Si

Downstream raw materials:

C35H55NO8

C41H69NO8Si

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