N-(but-3-en-1-yl)-N-(prop-2-yn-1-yl) 4-nitrobenzenesulfonamide

Base Information

• Chemical Name: N-(but-3-en-1-yl)-N-(prop-2-yn-1-yl) 4-nitrobenzenesulfonamide
• CAS No.: 1190202-61-9
• Molecular Formula: C₁₂H₁₂N₂O₄S
• Molecular Weight: 280.304
• Mol file: 1190202-61-9.mol

Synonyms:N-(but-3-en-1-yl)-N-(prop-2-yn-1-yl) 4-nitrobenzenesulfonamide

Chemical Property of N-(but-3-en-1-yl)-N-(prop-2-yn-1-yl) 4-nitrobenzenesulfonamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of N-(but-3-en-1-yl)-N-(prop-2-yn-1-yl) 4-nitrobenzenesulfonamide

There total 2 articles about N-(but-3-en-1-yl)-N-(prop-2-yn-1-yl) 4-nitrobenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

homoalylic alcohol (627-27-0) + C8H6N2O4S → N-(but-3-en-1-yl)-N-(prop-2-yn-1-yl) 4-nitrobenzenesulfonamide (1190202-61-9)

Guidance literature:

With azodicarboxylic acid bis(2-methoxyethyl) ester; triphenylphosphine; In tetrahydrofuran; at 20 ℃; Inert atmosphere;

DOI:10.1080/00397911.2017.1337151

Reference yield:

C21H32N2O4SSi → N-(but-3-en-1-yl)-N-(prop-2-yn-1-yl) 4-nitrobenzenesulfonamide (1190202-61-9)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 ℃; Inert atmosphere;

DOI:10.1021/ol901860b

Reference yield: 90.0%

N-(but-3-en-1-yl)-N-(prop-2-yn-1-yl) 4-nitrobenzenesulfonamide (1190202-61-9) → N-(but-3-en-1-yl)-N-(prop-2-yn-1-yl) 4-aminobenzenesulfonamide

Guidance literature:

With iron; ammonium chloride; In ethanol; water; at 20 ℃; for 72h;

DOI:10.1080/00397911.2017.1337151

upstream raw materials:

homoalylic alcohol

Downstream raw materials:

C₁₇H₁₈N₂O₈S