Benzyl-3-O-benzyl-4-O-(methyl-3,4-di-O-acetyl-2-desoxy-2-iod-β-D-glucopyranuronatosyl)-2-desoxy-α-D-arabino-hexopyranosid

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Chemical Name:Benzyl-3-O-benzyl-4-O-(methyl-3,4-di-O-acetyl-2-desoxy-2-iod-β-D-glucopyranuronatosyl)-2-desoxy-α-D-arabino-hexopyranosid
CAS No.:100603-99-4
Molecular Formula:C₃₁H₃₇IO₁₂
Molecular Weight:728.532
Hs Code.:

Synonyms:Benzyl-3-O-benzyl-4-O-(methyl-3,4-di-O-acetyl-2-desoxy-2-iod-β-D-glucopyranuronatosyl)-2-desoxy-α-D-arabino-hexopyranosid

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Chemical Property of Benzyl-3-O-benzyl-4-O-(methyl-3,4-di-O-acetyl-2-desoxy-2-iod-β-D-glucopyranuronatosyl)-2-desoxy-α-D-arabino-hexopyranosid

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Technology Process of Benzyl-3-O-benzyl-4-O-(methyl-3,4-di-O-acetyl-2-desoxy-2-iod-β-D-glucopyranuronatosyl)-2-desoxy-α-D-arabino-hexopyranosid

There total 2 articles about Benzyl-3-O-benzyl-4-O-(methyl-3,4-di-O-acetyl-2-desoxy-2-iod-β-D-glucopyranuronatosyl)-2-desoxy-α-D-arabino-hexopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.5%

: 100603-97-2
1,6-Anhydro-3-O-benzyl-4-O-(methyl-3,4-di-O-acetyl-2-desoxy-2-iod-β-D-glucopyranuronatosyl)-2-desoxy-β-D-arabino-hexopyranose

: 100-51-6,185532-71-2
benzyl alcohol

: 100604-00-0
Benzyl-3-O-benzyl-4-O-(methyl-3,4-di-O-acetyl-2-desoxy-2-iod-β-D-glucopyranuronatosyl)-2-desoxy-β-D-arabino-hexopyranosid

: 100603-99-4
Benzyl-3-O-benzyl-4-O-(methyl-3,4-di-O-acetyl-2-desoxy-2-iod-β-D-glucopyranuronatosyl)-2-desoxy-α-D-arabino-hexopyranosid

Guidance literature:: trifluoroacetic acid; at 80 ℃; for 6h;
DOI:10.1002/jlac.198619860609

Reference yield:

: 57690-62-7
methyl 3,4-di-O-acetyl-1,2-dideoxy-D-arabino-hex-1-enopyranuronate

: 100603-99-4
Benzyl-3-O-benzyl-4-O-(methyl-3,4-di-O-acetyl-2-desoxy-2-iod-β-D-glucopyranuronatosyl)-2-desoxy-α-D-arabino-hexopyranosid

Guidance literature:: Multi-step reaction with 2 steps

1: N-iodosuccinimide / acetonitrile / 24 h / Ambient temperature

2: 43.5 mg / TFA / 6 h / 80 °C

With N-iodo-succinimide; trifluoroacetic acid; In acetonitrile;
DOI:10.1002/jlac.198619860609