Technology Process of C24H38N2O5
There total 5 articles about C24H38N2O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine;
In
acetonitrile;
at 0 - 20 ℃;
for 16.25h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: potassium carbonate / N,N-dimethyl-formamide; tetrahydrofuran / 64 h / 70 °C
2.1: caesium carbonate / dichloromethane / 30 h / 42 °C
3.1: magnesium / iodine / diethyl ether / 2.75 h / Inert atmosphere; Reflux
3.2: 2 h / -78 - 20 °C
3.3: 1 h / 0 - 20 °C
4.1: hydrogenchloride / 1,4-dioxane; methanol / 1.5 h / 20 °C
5.1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / acetonitrile / 16.25 h / 0 - 20 °C
With
hydrogenchloride; potassium carbonate; benzotriazol-1-ol; caesium carbonate; magnesium; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine;
iodine;
In
tetrahydrofuran; 1,4-dioxane; methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: caesium carbonate / dichloromethane / 30 h / 42 °C
2.1: magnesium / iodine / diethyl ether / 2.75 h / Inert atmosphere; Reflux
2.2: 2 h / -78 - 20 °C
2.3: 1 h / 0 - 20 °C
3.1: hydrogenchloride / 1,4-dioxane; methanol / 1.5 h / 20 °C
4.1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / acetonitrile / 16.25 h / 0 - 20 °C
With
hydrogenchloride; benzotriazol-1-ol; caesium carbonate; magnesium; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine;
iodine;
In
1,4-dioxane; methanol; diethyl ether; dichloromethane; acetonitrile;