(1S,2S)-N-{N-[2-(4-methylcyclohexa-1,4-dienyl)ethyl]-N-methylsulfamoyl}-1,2-diphenylethylenediamine

Base Information

Chemical Name:(1S,2S)-N-{N-[2-(4-methylcyclohexa-1,4-dienyl)ethyl]-N-methylsulfamoyl}-1,2-diphenylethylenediamine
CAS No.:1427565-81-8
Molecular Formula:C₂₄H₃₁N₃O₂S
Molecular Weight:425.595
Hs Code.:

Synonyms:(1S,2S)-N-{N-[2-(4-methylcyclohexa-1,4-dienyl)ethyl]-N-methylsulfamoyl}-1,2-diphenylethylenediamine

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Chemical Property of (1S,2S)-N-{N-[2-(4-methylcyclohexa-1,4-dienyl)ethyl]-N-methylsulfamoyl}-1,2-diphenylethylenediamine

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Technology Process of (1S,2S)-N-{N-[2-(4-methylcyclohexa-1,4-dienyl)ethyl]-N-methylsulfamoyl}-1,2-diphenylethylenediamine

There total 3 articles about (1S,2S)-N-{N-[2-(4-methylcyclohexa-1,4-dienyl)ethyl]-N-methylsulfamoyl}-1,2-diphenylethylenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1427565-80-7
1-{N-[2-(4-methylcyclohexa-1,4-dienyl)ethyl]-N-methylsulfamoyl}-2,3-dimethylimidazolium triflate

: 29841-69-8
(S,S)-1,2-diphenyl-1,2-diaminoethane

: 1427565-81-8
(1S,2S)-N-{N-[2-(4-methylcyclohexa-1,4-dienyl)ethyl]-N-methylsulfamoyl}-1,2-diphenylethylenediamine

Guidance literature:: In acetonitrile; at 50 ℃;
DOI:10.1021/ol400393j

Reference yield:

: 1427565-75-0
N-[2-(4-methyl-cyclohexa-1,4-dienyl)ethyl]methylamine

: 1427565-81-8
(1S,2S)-N-{N-[2-(4-methylcyclohexa-1,4-dienyl)ethyl]-N-methylsulfamoyl}-1,2-diphenylethylenediamine

Guidance literature:: Multi-step reaction with 3 steps

1: acetonitrile / 6 h / 20 °C

2: dichloromethane / 3.17 h / -5 - 0 °C

3: acetonitrile / 50 °C

In dichloromethane; acetonitrile;
DOI:10.1021/ol400393j

Reference yield:

: 1427565-77-2
1-{N-[2-(4-methylcyclohexa-1,4-dienyl)ethyl]-N-methylsulfamoyl}-2-methylimidazole

: 1427565-81-8
(1S,2S)-N-{N-[2-(4-methylcyclohexa-1,4-dienyl)ethyl]-N-methylsulfamoyl}-1,2-diphenylethylenediamine

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 3.17 h / -5 - 0 °C

2: acetonitrile / 50 °C

In dichloromethane; acetonitrile;
DOI:10.1021/ol400393j