1-{N-[2-(4-methylcyclohexa-1,4-dienyl)ethyl]-N-methylsulfamoyl}-2-methylimidazole

Base Information

Chemical Name:1-{N-[2-(4-methylcyclohexa-1,4-dienyl)ethyl]-N-methylsulfamoyl}-2-methylimidazole
CAS No.:1427565-77-2
Molecular Formula:C₁₄H₂₁N₃O₂S
Molecular Weight:295.406
Hs Code.:

Synonyms:1-{N-[2-(4-methylcyclohexa-1,4-dienyl)ethyl]-N-methylsulfamoyl}-2-methylimidazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-{N-[2-(4-methylcyclohexa-1,4-dienyl)ethyl]-N-methylsulfamoyl}-2-methylimidazole

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Technology Process of 1-{N-[2-(4-methylcyclohexa-1,4-dienyl)ethyl]-N-methylsulfamoyl}-2-methylimidazole

There total 1 articles about 1-{N-[2-(4-methylcyclohexa-1,4-dienyl)ethyl]-N-methylsulfamoyl}-2-methylimidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1427565-75-0
N-[2-(4-methyl-cyclohexa-1,4-dienyl)ethyl]methylamine

: 2,3-dimethyl-1-[(2-methyl-1H-imidazol-1-yl)sulfonyl]-1H-imidazol-3-ium trifluoromethanesulfonate

: 1427565-77-2
1-{N-[2-(4-methylcyclohexa-1,4-dienyl)ethyl]-N-methylsulfamoyl}-2-methylimidazole

Guidance literature:: In acetonitrile; at 20 ℃; for 6h;
DOI:10.1021/ol400393j

Reference yield:

: 1427565-77-2
1-{N-[2-(4-methylcyclohexa-1,4-dienyl)ethyl]-N-methylsulfamoyl}-2-methylimidazole

: 333-27-7
methyl trifluoromethanesulfonate

: 1427565-80-7
1-{N-[2-(4-methylcyclohexa-1,4-dienyl)ethyl]-N-methylsulfamoyl}-2,3-dimethylimidazolium triflate

Guidance literature:: In dichloromethane; at -5 - 0 ℃; for 3.16667h;
DOI:10.1021/ol400393j

Reference yield:

: 1427565-77-2
1-{N-[2-(4-methylcyclohexa-1,4-dienyl)ethyl]-N-methylsulfamoyl}-2-methylimidazole

: 1427565-81-8
(1S,2S)-N-{N-[2-(4-methylcyclohexa-1,4-dienyl)ethyl]-N-methylsulfamoyl}-1,2-diphenylethylenediamine

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane / 3.17 h / -5 - 0 °C

2: acetonitrile / 50 °C

In dichloromethane; acetonitrile;
DOI:10.1021/ol400393j