phenyl 2-O-benzyl-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-L-glycero-1-thio-α-D-mannoheptopyranoside

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Chemical Name:phenyl 2-O-benzyl-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-L-glycero-1-thio-α-D-mannoheptopyranoside
CAS No.:1060735-36-5
Molecular Formula:C₂₆H₃₄O₈S
Molecular Weight:506.617
Hs Code.:

Synonyms:phenyl 2-O-benzyl-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-L-glycero-1-thio-α-D-mannoheptopyranoside

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Chemical Property of phenyl 2-O-benzyl-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-L-glycero-1-thio-α-D-mannoheptopyranoside

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Technology Process of phenyl 2-O-benzyl-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-L-glycero-1-thio-α-D-mannoheptopyranoside

There total 1 articles about phenyl 2-O-benzyl-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-L-glycero-1-thio-α-D-mannoheptopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1060735-28-5
phenyl 2-O-benzyl-6,7-dideoxy-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-1-thio-α-D-mannohepto-6-enopyranoside

: 1060735-32-1
phenyl 2-O-benzyl-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-D-glycero-1-thio-α-D-mannoheptopyranoside

: 1060735-36-5
phenyl 2-O-benzyl-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-L-glycero-1-thio-α-D-mannoheptopyranoside

Guidance literature:: With osmium(VIII) oxide; (8a,9R,8′′′a,9′′′R)-9,9′-[(2,5-diphenylpyrimidine-4,6-diyl)bis(oxy)]bis(6′-methoxy-10,11-dihydrocinchonan); water; potassium carbonate; potassium hexacyanoferrate(III); In toluene; tert-butyl alcohol; at 0 ℃; for 48h; optical yield given as %de;
DOI:10.1021/jo801414c

Reference yield: 91.0%

: 1060735-36-5
phenyl 2-O-benzyl-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-L-glycero-1-thio-α-D-mannoheptopyranoside

: 100-39-0
benzyl bromide

: 1060735-40-1
phenyl 2,7-di-O-benzyl-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-L-glycero-1-thio-α-D-mannoheptopyranoside

Guidance literature:: phenyl 2-O-benzyl-3,4-O-(2',3'-dimethoxybutane-2',3'-diyl)-L-glycero-1-thio-α-D-mannoheptopyranoside; With di(n-butyl)tin oxide; In toluene; for 2h; Reflux;

benzyl bromide; With cesium fluoride; In N,N-dimethyl-formamide; at 20 ℃; for 16h;
DOI:10.1021/jo801414c