methyl (2R,3S)-2-[(S)-2-benzyloxy-1-methylethyl]-3-[(S(S))-tert-butylsulfinylamino]-6-methylenedecanoate

Base Information

Chemical Name:methyl (2R,3S)-2-[(S)-2-benzyloxy-1-methylethyl]-3-[(S(S))-tert-butylsulfinylamino]-6-methylenedecanoate
CAS No.:1170688-92-2
Molecular Formula:C₂₆H₄₃NO₄S
Molecular Weight:465.698
Hs Code.:

Synonyms:methyl (2R,3S)-2-[(S)-2-benzyloxy-1-methylethyl]-3-[(S(S))-tert-butylsulfinylamino]-6-methylenedecanoate

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Chemical Property of methyl (2R,3S)-2-[(S)-2-benzyloxy-1-methylethyl]-3-[(S(S))-tert-butylsulfinylamino]-6-methylenedecanoate

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Technology Process of methyl (2R,3S)-2-[(S)-2-benzyloxy-1-methylethyl]-3-[(S(S))-tert-butylsulfinylamino]-6-methylenedecanoate

There total 1 articles about methyl (2R,3S)-2-[(S)-2-benzyloxy-1-methylethyl]-3-[(S(S))-tert-butylsulfinylamino]-6-methylenedecanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 258265-79-1
methyl (S)-4-(benzyloxy)-3-methylbutanoate

: 1170688-91-1
(S(S))-N-(tert-butylsulfinyl)-4-methyleneoctanimine

: methyl 2-(2-benzyloxy-1-methylethyl)-3-(tert-butylsulfinylamino)-6-methylenedecanoate

: 1170688-92-2
methyl (2R,3S)-2-[(S)-2-benzyloxy-1-methylethyl]-3-[(S(S))-tert-butylsulfinylamino]-6-methylenedecanoate

Guidance literature:: methyl (S)-4-(benzyloxy)-3-methylbutanoate; With lithium diisopropyl amide; In tetrahydrofuran; hexane; at -78 ℃; for 1h; Inert atmosphere;

With triisopropoxytitanium(IV) chloride; In tetrahydrofuran; hexane; at -78 ℃; for 1h; Inert atmosphere;

(S(S))-N-(tert-butylsulfinyl)-4-methyleneoctanimine; stereoselective reaction; Further stages;
DOI:10.1016/j.tetasy.2009.03.002