3-O-MEM-6-O-TrO-PEG₄-nalbuphine

Base Information

Chemical Name:3-O-MEM-6-O-TrO-PEG₄-nalbuphine
CAS No.:1056881-15-2
Molecular Formula:C₅₂H₆₅NO₁₀
Molecular Weight:864.089
Hs Code.:

3-O-MEM-6-O-TrO-PEG<sub>4</sub>-nalbuphine

Synonyms:3-O-MEM-6-O-TrO-PEG₄-nalbuphine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-O-MEM-6-O-TrO-PEG₄-nalbuphine

Chemical Property:

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Technology Process of 3-O-MEM-6-O-TrO-PEG₄-nalbuphine

There total 3 articles about 3-O-MEM-6-O-TrO-PEG₄-nalbuphine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 20594-83-6
nalbuphine

: 1056881-15-2
3-O-MEM-6-O-TrO-PEG₄-nalbuphine

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / acetone; toluene / 21 h / 20 °C

2.1: sodium hydride / N,N-dimethyl-formamide; toluene / 22.5 h / 45 °C

2.2: 20 °C

With sodium hydride; potassium carbonate; In N,N-dimethyl-formamide; acetone; toluene;

Reference yield:

: 1056881-05-0
3-O-MEM-nalbuphine

: 146462-60-4
2-(2-(2-<2-(triphenylmethoxy)ethoxy>ethoxy)ethoxy)ethyl methanesulfonate

: 1056881-15-2
3-O-MEM-6-O-TrO-PEG₄-nalbuphine

Guidance literature:: 3-O-MEM-nalbuphine; 2-(2-(2-<2-(triphenylmethoxy)ethoxy>ethoxy)ethoxy)ethyl methanesulfonate; With sodium hydride; In N,N-dimethyl-formamide; toluene; at 45 ℃; for 22.5h;

With water; sodium chloride; In N,N-dimethyl-formamide; toluene; at 20 ℃;

Reference yield:

: 23277-43-2
nalbuphine hydrochloride

: 1056881-15-2
3-O-MEM-6-O-TrO-PEG₄-nalbuphine

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogenchloride; potassium carbonate; sodium chloride / water / pH 9.3

2.1: potassium carbonate / acetone; toluene / 21 h / 20 °C

3.1: sodium hydride / N,N-dimethyl-formamide; toluene / 22.5 h / 45 °C

3.2: 20 °C

With hydrogenchloride; sodium hydride; potassium carbonate; sodium chloride; In water; N,N-dimethyl-formamide; acetone; toluene;