homo-ent-secodrial

Base Information

Chemical Name:homo-ent-secodrial
CAS No.:1206911-02-5
Molecular Formula:C₂₇H₃₆O₆
Molecular Weight:456.579
Hs Code.:

Synonyms:homo-ent-secodrial

Suppliers and Price of homo-ent-secodrial

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of homo-ent-secodrial

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of homo-ent-secodrial

There total 3 articles about homo-ent-secodrial which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1206911-18-3
C₂₇H₃₈O₆

: 1206911-02-5
homo-ent-secodrial

Guidance literature:: With oxalyl dichloride; dimethyl sulfoxide; triethylamine; In dichloromethane; at -60 ℃; Inert atmosphere;
DOI:10.1002/ejoc.200901021

Reference yield:

: 1035948-08-3
C₁₆H₂₈O

: 1206911-02-5
homo-ent-secodrial

Guidance literature:: Multi-step reaction with 5 steps

1.1: tert-butyldimethylsilyl chloride

2.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 3 h / 25 °C / Inert atmosphere

2.2: 1 h / 25 °C / Inert atmosphere

3.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 2 h / 25 °C

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2.5 h / 20 °C

5.1: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / -60 °C / Inert atmosphere

With oxalyl dichloride; di-isopropyl azodicarboxylate; tetrabutyl ammonium fluoride; tert-butyldimethylsilyl chloride; dimethyl sulfoxide; triethylamine; 9-bora-bicyclo[3.3.1]nonane; triphenylphosphine; In tetrahydrofuran; dichloromethane; 3.1: Mitsunobu reaction / 5.1: Swern oxidation;
DOI:10.1002/ejoc.200901021

Reference yield:

: C₁₆H₂₆O₃

: 1206911-02-5
homo-ent-secodrial

Guidance literature:: Multi-step reaction with 7 steps

1.1: potassium tert-butylate / toluene / 0.75 h / 20 °C / Inert atmosphere; Cooling with ice

2.1: lithium aluminium tetrahydride

3.1: tert-butyldimethylsilyl chloride

4.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 3 h / 25 °C / Inert atmosphere

4.2: 1 h / 25 °C / Inert atmosphere

5.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 2 h / 25 °C

6.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2.5 h / 20 °C

7.1: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / -60 °C / Inert atmosphere

With lithium aluminium tetrahydride; oxalyl dichloride; di-isopropyl azodicarboxylate; potassium tert-butylate; tetrabutyl ammonium fluoride; tert-butyldimethylsilyl chloride; dimethyl sulfoxide; triethylamine; 9-bora-bicyclo[3.3.1]nonane; triphenylphosphine; In tetrahydrofuran; dichloromethane; toluene; 1.1: Wittig reaction / 5.1: Mitsunobu reaction / 7.1: Swern oxidation;
DOI:10.1002/ejoc.200901021