7,7,8,8-Tetracylohexyl-2,3:5,6-dibenzo-7,8-disilabicyclo<2.2.2>octa-2,5-dien

Base Information

Chemical Name:7,7,8,8-Tetracylohexyl-2,3:5,6-dibenzo-7,8-disilabicyclo<2.2.2>octa-2,5-dien
CAS No.:107352-14-7
Molecular Formula:C₃₈H₅₄Si₂
Molecular Weight:567.018
Hs Code.:

Synonyms:7,7,8,8-Tetracylohexyl-2,3:5,6-dibenzo-7,8-disilabicyclo<2.2.2>octa-2,5-dien

Suppliers and Price of 7,7,8,8-Tetracylohexyl-2,3:5,6-dibenzo-7,8-disilabicyclo<2.2.2>octa-2,5-dien

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 7,7,8,8-Tetracylohexyl-2,3:5,6-dibenzo-7,8-disilabicyclo<2.2.2>octa-2,5-dien

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 7,7,8,8-Tetracylohexyl-2,3:5,6-dibenzo-7,8-disilabicyclo<2.2.2>octa-2,5-dien

There total 3 articles about 7,7,8,8-Tetracylohexyl-2,3:5,6-dibenzo-7,8-disilabicyclo<2.2.2>octa-2,5-dien which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 120-12-7
anthracene

: 107352-11-4
1,1,2,2-Tetracyclohexyl-1,2-dichlordisilan

: 68750-07-2
1,1,2,2-tetracyclohexyldisilane

: 107352-14-7
7,7,8,8-Tetracylohexyl-2,3:5,6-dibenzo-7,8-disilabicyclo<2.2.2>octa-2,5-dien

Guidance literature:: With lithium; In 1,2-dimethoxyethane; for 16h; Ambient temperature;
DOI:10.1016/S0022-328X(00)99533-0

Reference yield:

: 68750-07-2
1,1,2,2-tetracyclohexyldisilane

: 107352-14-7
7,7,8,8-Tetracylohexyl-2,3:5,6-dibenzo-7,8-disilabicyclo<2.2.2>octa-2,5-dien

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / chlorine / petroleum ether / -60 °C

2: 33 percent / lithium / 1,2-dimethoxy-ethane / 16 h / Ambient temperature

With chlorine; lithium; In 1,2-dimethoxyethane; Petroleum ether;
DOI:10.1016/S0022-328X(00)99533-0

Reference yield:

: 2227-27-2
chlorodicyclohexylsilane

: 107352-14-7
7,7,8,8-Tetracylohexyl-2,3:5,6-dibenzo-7,8-disilabicyclo<2.2.2>octa-2,5-dien

Guidance literature:: Multi-step reaction with 3 steps

1: 77 percent / Kalium / 48 h

2: 88 percent / chlorine / petroleum ether / -60 °C

3: 33 percent / lithium / 1,2-dimethoxy-ethane / 16 h / Ambient temperature

With potassium; chlorine; lithium; In 1,2-dimethoxyethane; Petroleum ether;
DOI:10.1016/S0022-328X(00)99533-0