(5R)-3-{4-[5-(dimethoxymethyl)-1-methyl-1H-pyrazol-3-yl]phenyl}-5-(hydroxymethyl)-1,3-oxazolidin-2-one

Base Information

Chemical Name:(5R)-3-{4-[5-(dimethoxymethyl)-1-methyl-1H-pyrazol-3-yl]phenyl}-5-(hydroxymethyl)-1,3-oxazolidin-2-one
CAS No.:765287-12-5
Molecular Formula:C₁₇H₂₁N₃O₅
Molecular Weight:347.371
Hs Code.:

Synonyms:(5R)-3-{4-[5-(dimethoxymethyl)-1-methyl-1H-pyrazol-3-yl]phenyl}-5-(hydroxymethyl)-1,3-oxazolidin-2-one

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Chemical Property of (5R)-3-{4-[5-(dimethoxymethyl)-1-methyl-1H-pyrazol-3-yl]phenyl}-5-(hydroxymethyl)-1,3-oxazolidin-2-one

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Technology Process of (5R)-3-{4-[5-(dimethoxymethyl)-1-methyl-1H-pyrazol-3-yl]phenyl}-5-(hydroxymethyl)-1,3-oxazolidin-2-one

There total 1 articles about (5R)-3-{4-[5-(dimethoxymethyl)-1-methyl-1H-pyrazol-3-yl]phenyl}-5-(hydroxymethyl)-1,3-oxazolidin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 765287-11-4
benzyl 4-[5-(diethoxymethyl)-1-methyl-1H-pyrazol-3-yl]phenylcarbamate

: 60456-26-0
(R)-glycidyl butyrate

: 149-73-5
trimethyl orthoformate

: 765287-12-5
(5R)-3-{4-[5-(dimethoxymethyl)-1-methyl-1H-pyrazol-3-yl]phenyl}-5-(hydroxymethyl)-1,3-oxazolidin-2-one

Guidance literature:: benzyl 4-[5-(diethoxymethyl)-1-methyl-1H-pyrazol-3-yl]phenylcarbamate; With n-butyllithium; In tetrahydrofuran; hexanes; at -70 ℃; for 0.583333h;

(R)-glycidyl butyrate; In tetrahydrofuran; hexanes; at -70 - 20 ℃; for 16h;

trimethyl orthoformate; With (R)-10-camphorsulfonic acid; triethylamine; more than 3 stages;

Reference yield:

: 765287-12-5
(5R)-3-{4-[5-(dimethoxymethyl)-1-methyl-1H-pyrazol-3-yl]phenyl}-5-(hydroxymethyl)-1,3-oxazolidin-2-one

: 765287-13-6
3-{4-[(5R)-5-(azidomethyl)-2-oxo-1,3-oxazolidin-3-yl]phenyl}-1-methyl-1H-pyrazole-5-carbaldehyde

Guidance literature:: (5R)-3-{4-[5-(dimethoxymethyl)-1-methyl-1H-pyrazol-3-yl]phenyl}-5-(hydroxymethyl)-1,3-oxazolidin-2-one; With methanesulfonyl chloride; triethylamine; In tetrahydrofuran; dichloromethane; at 0 ℃; for 1h;

With sodium azide; 18-crown-6 ether; tetra-(n-butyl)ammonium iodide; In DMF (N,N-dimethyl-formamide); at 90 ℃; for 16h;

With water; trifluoroacetic acid; In dichloromethane; at 20 ℃; for 0.5h;