2-benzyloxy-6-bis-methylthiomethylpyridine

Base Information

• Chemical Name: 2-benzyloxy-6-bis-methylthiomethylpyridine
• CAS No.: 161807-31-4
• Molecular Formula: C₁₅H₁₇NOS₂
• Molecular Weight: 291.438

Synonyms:2-benzyloxy-6-bis-methylthiomethylpyridine

Chemical Property of 2-benzyloxy-6-bis-methylthiomethylpyridine

Chemical Property:

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Technology Process of 2-benzyloxy-6-bis-methylthiomethylpyridine

There total 2 articles about 2-benzyloxy-6-bis-methylthiomethylpyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

2-chloro-6-(bis-methylthiomethyl)pyridine (161807-29-0) + benzyl alcohol (100-51-6,185532-71-2) → 2-benzyloxy-6-bis-methylthiomethylpyridine (161807-31-4)

Guidance literature:

With potassium tert-butylate; In tert-butyl alcohol; at 120 ℃; for 48h;

DOI:10.1016/0040-4020(94)01020-Z

Reference yield:

6-chloro-2-picoline (18368-63-3) → 2-benzyloxy-6-bis-methylthiomethylpyridine (161807-31-4)

Guidance literature:

Multi-step reaction with 2 steps

1: n-BuLi / 1.) THF, hexane, -78 deg C, 5 h; 2.) THF, hexane, -78 deg, 5 h

2: 90 percent / K-t-BuO / 2-methyl-propan-2-ol / 48 h / 120 °C

With n-butyllithium; potassium tert-butylate; In tert-butyl alcohol;

DOI:10.1016/0040-4020(94)01020-Z

Reference yield: 100.0%

methyl vinyl ketone (78-94-4,25038-87-3) + 2-benzyloxy-6-bis-methylthiomethylpyridine (161807-31-4) → 4-<(6-benzyloxy-2-pyridyl)bis-methylthiomethyl>-2-butanone

Guidance literature:

With copper(l) iodide; n-butyllithium; In tetrahydrofuran; at -78 ℃; for 3h;

DOI:10.1016/0040-4020(94)01020-Z

upstream raw materials:

2-chloro-6-(bis-methylthiomethyl)pyridine

benzyl alcohol

6-chloro-2-picoline

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