nitrido{5,10,15,20-tetrakis(4-methylphenyl)porphinato}chromium(V)

Base Information

Chemical Name:nitrido{5,10,15,20-tetrakis(4-methylphenyl)porphinato}chromium(V)
CAS No.:84174-28-7
Molecular Formula:C₄₈H₃₆CrN₅
Molecular Weight:734.843
Hs Code.:

Synonyms:nitrido{5,10,15,20-tetrakis(4-methylphenyl)porphinato}chromium(V)

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Chemical Property of nitrido{5,10,15,20-tetrakis(4-methylphenyl)porphinato}chromium(V)

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Technology Process of nitrido{5,10,15,20-tetrakis(4-methylphenyl)porphinato}chromium(V)

There total 6 articles about nitrido{5,10,15,20-tetrakis(4-methylphenyl)porphinato}chromium(V) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: (acetone)aquaazido[tetra(p-tolyl)porphinato]chromium(III)

: 84174-28-7
[Cr(C₂₀N₄H₈(C₆H₄CH₃)4)N]

Guidance literature:: In toluene; byproducts: N2; Irradiation (UV/VIS); UV irradn. (high pressure Hg lamp), reflux, stirring, 2 h; filtering, evapn. in vac., chromy. (SiO2, toluene), crystn. from benzene;

Reference yield: 82.0%

: 43145-40-0
azido(5,10,15,20-tetra-p-tolylporphinato)chromium(III)

: 84174-28-7
nitrido{5,10,15,20-tetrakis(4-methylphenyl)porphinato}chromium(V)

Guidance literature:: In benzene; Complex was dissolved in benzene (stirrer, N2 bubbler). Soln. was irradiated for 2 h at 15°C.; Solvent was removed in vac., residue was dissolved in benzene, chromd.,soln. was concd., dried in vac., chromd., crystd. from benzene-pentane,dried in vac.; elem. anal.;

Reference yield: 55.0%

: C₂₀H₈N₄(C₆H₄CH₃)4Cr(OH)(H₂O)*H₂O

: 84174-28-7
nitrido{5,10,15,20-tetrakis(4-methylphenyl)porphinato}chromium(V)

: 80584-26-5
(5,10,15,20-tetra-p-tolylporphyrinato)oxochromium(IV)

Guidance literature:: With NH₃; NaOCl; In ethanol; dichloromethane; water; byproducts: H2O, NaCl; To soln. of complex in CH2Cl2/EtOH is added aq. NH3 and aq. NaOCl, mixt. was stirred for 3-4 h.; Mixt. is washed with H2O, organic phase is sepd. and evapd. in vac., residue is dissolved in toluene and chromd., soln. is filtered and dried in vac., residue is recrystd. from benzene; elem. anal.;