methyl 2-[(N-allyl-(2-trimethylsilyl)ethanesulfonylamino)(4-cyanophenyl)methyl]acrylate

Base Information

Chemical Name:methyl 2-[(N-allyl-(2-trimethylsilyl)ethanesulfonylamino)(4-cyanophenyl)methyl]acrylate
CAS No.:929012-41-9
Molecular Formula:C₂₀H₂₈N₂O₄SSi
Molecular Weight:420.605
Hs Code.:

Synonyms:methyl 2-[(N-allyl-(2-trimethylsilyl)ethanesulfonylamino)(4-cyanophenyl)methyl]acrylate

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Chemical Property of methyl 2-[(N-allyl-(2-trimethylsilyl)ethanesulfonylamino)(4-cyanophenyl)methyl]acrylate

Chemical Property:

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Technology Process of methyl 2-[(N-allyl-(2-trimethylsilyl)ethanesulfonylamino)(4-cyanophenyl)methyl]acrylate

There total 3 articles about methyl 2-[(N-allyl-(2-trimethylsilyl)ethanesulfonylamino)(4-cyanophenyl)methyl]acrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 929012-64-6
methyl 2-[(4-cyanophenyl)(2-trimethylsilyl)(ethanesulfonylamino)methyl]acrylate

: 106-95-6
allyl bromide

: 929012-41-9
methyl 2-[(N-allyl-(2-trimethylsilyl)ethanesulfonylamino)(4-cyanophenyl)methyl]acrylate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 6h;
DOI:10.1021/jo062239p

Reference yield:

: 125486-96-6
2-(trimethylsilyl)ethanesulfonamide

: 929012-41-9
methyl 2-[(N-allyl-(2-trimethylsilyl)ethanesulfonylamino)(4-cyanophenyl)methyl]acrylate

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / DABCO / propan-2-ol / 6 h / 70 °C

2: 98 percent / potassium carbonate / dimethylformamide / 6 h / 20 °C

With 1,4-diaza-bicyclo[2.2.2]octane; potassium carbonate; In N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1021/jo062239p

Reference yield:

: 105-07-7
4-cyanobenzaldehyde

: 929012-41-9
methyl 2-[(N-allyl-(2-trimethylsilyl)ethanesulfonylamino)(4-cyanophenyl)methyl]acrylate

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / DABCO / propan-2-ol / 6 h / 70 °C

2: 98 percent / potassium carbonate / dimethylformamide / 6 h / 20 °C

With 1,4-diaza-bicyclo[2.2.2]octane; potassium carbonate; In N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1021/jo062239p