methyl 2-[(4-cyanophenyl)(2-trimethylsilyl)(ethanesulfonylamino)methyl]acrylate

Base Information

Chemical Name:methyl 2-[(4-cyanophenyl)(2-trimethylsilyl)(ethanesulfonylamino)methyl]acrylate
CAS No.:929012-64-6
Molecular Formula:C₁₇H₂₄N₂O₄SSi
Molecular Weight:380.54
Hs Code.:

Synonyms:methyl 2-[(4-cyanophenyl)(2-trimethylsilyl)(ethanesulfonylamino)methyl]acrylate

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Chemical Property of methyl 2-[(4-cyanophenyl)(2-trimethylsilyl)(ethanesulfonylamino)methyl]acrylate

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Technology Process of methyl 2-[(4-cyanophenyl)(2-trimethylsilyl)(ethanesulfonylamino)methyl]acrylate

There total 1 articles about methyl 2-[(4-cyanophenyl)(2-trimethylsilyl)(ethanesulfonylamino)methyl]acrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 125486-96-6
2-(trimethylsilyl)ethanesulfonamide

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: 105-07-7
4-cyanobenzaldehyde

: 929012-64-6
methyl 2-[(4-cyanophenyl)(2-trimethylsilyl)(ethanesulfonylamino)methyl]acrylate

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; In isopropyl alcohol; at 70 ℃; for 6h;
DOI:10.1021/jo062239p

Reference yield: 98.0%

: 929012-64-6
methyl 2-[(4-cyanophenyl)(2-trimethylsilyl)(ethanesulfonylamino)methyl]acrylate

: 106-95-6
allyl bromide

: 929012-41-9
methyl 2-[(N-allyl-(2-trimethylsilyl)ethanesulfonylamino)(4-cyanophenyl)methyl]acrylate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 6h;
DOI:10.1021/jo062239p

Reference yield:

: 929012-64-6
methyl 2-[(4-cyanophenyl)(2-trimethylsilyl)(ethanesulfonylamino)methyl]acrylate

: 929012-42-0
methyl 2-((4-cyanophenyl)-1-(2-trimethylsilyl)-ethanesulfonyl)-2,5-dihydro-1H-pyrrole-3-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / potassium carbonate / dimethylformamide / 6 h / 20 °C

2: 90 percent / 2nd generation Grubbs catalyst / CH₂Cl₂ / 20 °C

With potassium carbonate; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In dichloromethane; N,N-dimethyl-formamide; 2: olefin metathesis;
DOI:10.1021/jo062239p