2-[4-fluoro-2-(2-oxo-1,2-diphenylethylideneamino)phenylimino]-1,2-diphenylethanone

Base Information

Chemical Name:2-[4-fluoro-2-(2-oxo-1,2-diphenylethylideneamino)phenylimino]-1,2-diphenylethanone
CAS No.:1316847-11-6
Molecular Formula:C₃₄H₂₃FN₂O₂
Molecular Weight:510.567
Hs Code.:

Synonyms:2-[4-fluoro-2-(2-oxo-1,2-diphenylethylideneamino)phenylimino]-1,2-diphenylethanone

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Chemical Property of 2-[4-fluoro-2-(2-oxo-1,2-diphenylethylideneamino)phenylimino]-1,2-diphenylethanone

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Technology Process of 2-[4-fluoro-2-(2-oxo-1,2-diphenylethylideneamino)phenylimino]-1,2-diphenylethanone

There total 1 articles about 2-[4-fluoro-2-(2-oxo-1,2-diphenylethylideneamino)phenylimino]-1,2-diphenylethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 367-31-7
4-fluoro-1,2-phenylenediamine

: 134-81-6
benzil

: 1316847-11-6
2-[4-fluoro-2-(2-oxo-1,2-diphenylethylideneamino)phenylimino]-1,2-diphenylethanone

Guidance literature:: In ethanol; Reflux;
DOI:10.1016/j.saa.2011.03.057

Reference yield: 73.0%

: 367-31-7
4-fluoro-1,2-phenylenediamine

: 1316847-11-6
2-[4-fluoro-2-(2-oxo-1,2-diphenylethylideneamino)phenylimino]-1,2-diphenylethanone

: palladium dichloride

: Pd(C₆H₃F(NC(C₆H₅)C(N)C₆H₅)2C₆H₃F)⁽²⁺⁾*2Cl^(1-)=[Pd(C₆H₃F(NC(C₆H₅)C(N)C₆H₅)2C₆H₃F)]Cl₂

Guidance literature:: In methanol; solns. of ligands in MeOH were mixed with PdCl2; mixt. boiled under reflux for about 7-8 h on a radio head; mixt. concd.; kept at room temp. overnight; solid washed (MeOH); dried (vac.); recrystd. (MeOH/C6H6, 1:1); elem. anal.;
DOI:10.1016/j.saa.2011.03.057

Reference yield: 67.0%

: 1316847-11-6
2-[4-fluoro-2-(2-oxo-1,2-diphenylethylideneamino)phenylimino]-1,2-diphenylethanone

: 95-54-5
1,2-diamino-benzene

: palladium dichloride

: Pd(C₆H₃F(NC(C₆H₅)C(N)C₆H₅)2C₆H₄)⁽²⁺⁾*2Cl^(1-)=[Pd(C₆H₃F(NC(C₆H₅)C(N)C₆H₅)2C₆H₄)]Cl₂

Guidance literature:: In methanol; solns. of ligands in MeOH were mixed with PdCl2; mixt. boiled under reflux for about 7-8 h on a radio head; mixt. concd.; kept at room temp.; solid washed (MeOH); dried (vac.); recrystd. (MeOH/C6H6, 1:1); elem. anal.;
DOI:10.1016/j.saa.2011.03.057