4-Azido-benzoic acid (3aR,4R,6R,6aR)-6-methoxy-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester

Base Information

Chemical Name:4-Azido-benzoic acid (3aR,4R,6R,6aR)-6-methoxy-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester
CAS No.:76479-98-6
Molecular Formula:C₁₆H₁₉N₃O₆
Molecular Weight:349.343
Hs Code.:

Synonyms:4-Azido-benzoic acid (3aR,4R,6R,6aR)-6-methoxy-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester

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Chemical Property of 4-Azido-benzoic acid (3aR,4R,6R,6aR)-6-methoxy-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester

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Technology Process of 4-Azido-benzoic acid (3aR,4R,6R,6aR)-6-methoxy-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester

There total 5 articles about 4-Azido-benzoic acid (3aR,4R,6R,6aR)-6-methoxy-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 76479-97-5
methyl 2,3-O-isopropylidene-5-O-(p-nitrobenzoyl)-β-D-ribofuranoside

: 6427-66-3
4-azidobenzoic acid

: 76480-02-9
4-Amino-benzoic acid (3aR,4R,6R,6aR)-6-methoxy-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester

: 76479-98-6
4-Azido-benzoic acid (3aR,4R,6R,6aR)-6-methoxy-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester

: 76480-00-7
C₃₂H₃₈N₂O₁₂

: 62-23-7
4-nitro-benzoic acid

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; at 150 ℃; for 3h; Product distribution; Mechanism; other reaction times and solvents; other nitrobenzoates;
DOI:10.1021/jo00321a022

Reference yield:

: 76479-97-5
methyl 2,3-O-isopropylidene-5-O-(p-nitrobenzoyl)-β-D-ribofuranoside

: 6427-66-3
4-azidobenzoic acid

: 76480-02-9
4-Amino-benzoic acid (3aR,4R,6R,6aR)-6-methoxy-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester

: 76479-98-6
4-Azido-benzoic acid (3aR,4R,6R,6aR)-6-methoxy-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester

: 76480-00-7
C₃₂H₃₈N₂O₁₂

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; at 150 ℃; for 3h; Further byproducts given. Title compound not separated from byproducts;
DOI:10.1021/jo00321a022

Reference yield:

: 76479-97-5
methyl 2,3-O-isopropylidene-5-O-(p-nitrobenzoyl)-β-D-ribofuranoside

: 76480-02-9
4-Amino-benzoic acid (3aR,4R,6R,6aR)-6-methoxy-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester

: 76479-98-6
4-Azido-benzoic acid (3aR,4R,6R,6aR)-6-methoxy-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester

: 76480-00-7
C₃₂H₃₈N₂O₁₂

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; at 150 ℃; for 2h; Title compound not separated from byproducts;
DOI:10.1021/jo00321a022