1,1,1,3,3,3-hexafluoro-2,2-bis-[4-methyl-3-(2,2,2-trifluoro-1-methanesulfonyloxy-1-trifluoromethyl-ethyl)-phenyl]-propane

Base Information

Chemical Name:1,1,1,3,3,3-hexafluoro-2,2-bis-[4-methyl-3-(2,2,2-trifluoro-1-methanesulfonyloxy-1-trifluoromethyl-ethyl)-phenyl]-propane
CAS No.:127002-51-1
Molecular Formula:C₂₅H₁₈F₁₈O₆S₂
Molecular Weight:820.518
Hs Code.:

Synonyms:1,1,1,3,3,3-hexafluoro-2,2-bis-[4-methyl-3-(2,2,2-trifluoro-1-methanesulfonyloxy-1-trifluoromethyl-ethyl)-phenyl]-propane

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Chemical Property of 1,1,1,3,3,3-hexafluoro-2,2-bis-[4-methyl-3-(2,2,2-trifluoro-1-methanesulfonyloxy-1-trifluoromethyl-ethyl)-phenyl]-propane

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Technology Process of 1,1,1,3,3,3-hexafluoro-2,2-bis-[4-methyl-3-(2,2,2-trifluoro-1-methanesulfonyloxy-1-trifluoromethyl-ethyl)-phenyl]-propane

There total 3 articles about 1,1,1,3,3,3-hexafluoro-2,2-bis-[4-methyl-3-(2,2,2-trifluoro-1-methanesulfonyloxy-1-trifluoromethyl-ethyl)-phenyl]-propane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 127002-42-0
1,1,1,3,3,3-hexafluoro-2,2-bis-[4-methyl-3-(2,2,2-trifluoro-1-hydroxy-1-trifluoromethyl-ethyl)-phenyl]-propane

: 124-63-0
methanesulfonyl chloride

: 127002-51-1
1,1,1,3,3,3-hexafluoro-2,2-bis-[4-methyl-3-(2,2,2-trifluoro-1-methanesulfonyloxy-1-trifluoromethyl-ethyl)-phenyl]-propane

Guidance literature:: With triethylamine; In dichloromethane; for 2h; -5 deg C to RT;
DOI:10.1021/jo00301a044

Reference yield:

: 1095-77-8
1,1,1,3,3,3-hexafluoro-2,2-di(p-tolyl)propane

: 127002-51-1
1,1,1,3,3,3-hexafluoro-2,2-bis-[4-methyl-3-(2,2,2-trifluoro-1-methanesulfonyloxy-1-trifluoromethyl-ethyl)-phenyl]-propane

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / Br₂, Fe / CCl₄ / 1 h / 25 °C

2: 1) Mg / 1) ether, 2h, reflux, 2) -78 deg C

3: 75 percent / NEt₃ / CH₂Cl₂ / 2 h / -5 deg C to RT

With bromine; iron; magnesium; triethylamine; In tetrachloromethane; dichloromethane;
DOI:10.1021/jo00301a044

Reference yield:

: 127002-41-9
C₁₇H₁₂Br₂F₆

: 127002-51-1
1,1,1,3,3,3-hexafluoro-2,2-bis-[4-methyl-3-(2,2,2-trifluoro-1-methanesulfonyloxy-1-trifluoromethyl-ethyl)-phenyl]-propane

Guidance literature:: Multi-step reaction with 2 steps

1: 1) Mg / 1) ether, 2h, reflux, 2) -78 deg C

2: 75 percent / NEt₃ / CH₂Cl₂ / 2 h / -5 deg C to RT

With magnesium; triethylamine; In dichloromethane;
DOI:10.1021/jo00301a044