C₁₆H₁₃ClN₄

Base Information

• Chemical Name: C₁₆H₁₃ClN₄
• CAS No.: 1421321-99-4
• Molecular Formula: C₁₆H₁₃ClN₄
• Molecular Weight: 296.759
• Mol file: 1421321-99-4.mol

Synonyms:C₁₆H₁₃ClN₄

Chemical Property of C₁₆H₁₃ClN₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₆H₁₃ClN₄

There total 2 articles about C₁₆H₁₃ClN₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

6-amino-3,4-dihydro-1H-quinolin-2-one (22246-13-5) → C16H13ClN4 (1421321-99-4)

Guidance literature:

Multi-step reaction with 2 steps

1: tetraphosphorus decasulfide; triethylamine / acetonitrile

2: cyclohexanol / 6 h / Reflux; Inert atmosphere

With tetraphosphorus decasulfide; triethylamine; In acetonitrile; cyclohexanol;

DOI:10.1016/j.bmcl.2012.11.078

Reference yield:

C9H10N2S (708983-83-9) + 3-chlorobenzhydrazide (1673-47-8) → C16H13ClN4 (1421321-99-4)

Guidance literature:

In cyclohexanol; for 6h; Reflux; Inert atmosphere;

DOI:10.1016/j.bmcl.2012.11.078

Reference yield:

C16H13ClN4 (1421321-99-4) → C29H28Cl2N6O (1421322-07-7)

Guidance literature:

Multi-step reaction with 2 steps

1: dichloromethane / 20 °C

2: potassium carbonate / acetone / 10 h / Reflux

With potassium carbonate; In dichloromethane; acetone;

DOI:10.1016/j.bmcl.2012.11.078

upstream raw materials:

6-amino-3,4-dihydro-1H-quinolin-2-one

C₉H₁₀N₂S

3-chlorobenzhydrazide

Downstream raw materials:

C₁₈H₁₄Cl₂N₄O

C₂₉H₂₈ClFN₆O

C₂₉H₂₈ClFN₆O

C₂₉H₂₈ClFN₆O

Refernces