Technology Process of C9H6BrF3O4
There total 5 articles about C9H6BrF3O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C8H5BrF3IO2;
With
isopropylmagnesium chloride; lithium chloride;
In
tetrahydrofuran;
at -78 ℃;
for 1h;
carbon dioxide;
In
tetrahydrofuran;
at -78 - 20 ℃;
for 2h;
With
hydrogenchloride;
In
tetrahydrofuran; water;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: pyridinium hydrobromide perbromide / dichloromethane / 1 h / 0 °C
2.1: hydrogenchloride; sodium nitrite / 1,4-dioxane; water / 0.5 h / 20 °C
2.2: 72 h / 0 - 20 °C
3.1: isopropylmagnesium chloride; lithium chloride / tetrahydrofuran / 1 h / -78 °C
3.2: 2 h / -78 - 20 °C
With
hydrogenchloride; isopropylmagnesium chloride; pyridinium hydrobromide perbromide; lithium chloride; sodium nitrite;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane; water;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium dithionite; water / tetrahydrofuran / 16 h / 20 °C
2.1: pyridinium hydrobromide perbromide / dichloromethane / 1 h / 0 °C
3.1: hydrogenchloride; sodium nitrite / 1,4-dioxane; water / 0.5 h / 20 °C
3.2: 72 h / 0 - 20 °C
4.1: isopropylmagnesium chloride; lithium chloride / tetrahydrofuran / 1 h / -78 °C
4.2: 2 h / -78 - 20 °C
With
hydrogenchloride; sodium dithionite; water; isopropylmagnesium chloride; pyridinium hydrobromide perbromide; lithium chloride; sodium nitrite;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane; water;
