N-(6-(2-hydroxybut-3-en-2-yl)benzo[d][1,3]dioxol-5-yl)-4-methylbenzenesulfonamide

Base Information

Chemical Name:N-(6-(2-hydroxybut-3-en-2-yl)benzo[d][1,3]dioxol-5-yl)-4-methylbenzenesulfonamide
CAS No.:1178907-41-9
Molecular Formula:C₁₈H₁₉NO₅S
Molecular Weight:361.419
Hs Code.:

Synonyms:N-(6-(2-hydroxybut-3-en-2-yl)benzo[d][1,3]dioxol-5-yl)-4-methylbenzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(6-(2-hydroxybut-3-en-2-yl)benzo[d][1,3]dioxol-5-yl)-4-methylbenzenesulfonamide

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Technology Process of N-(6-(2-hydroxybut-3-en-2-yl)benzo[d][1,3]dioxol-5-yl)-4-methylbenzenesulfonamide

There total 1 articles about N-(6-(2-hydroxybut-3-en-2-yl)benzo[d][1,3]dioxol-5-yl)-4-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1826-67-1
vinyl magnesium bromide

: 460994-52-9
N-(6-acetylbenzo[d][1,3]dioxol-5-yl)-4-methylbenzenesulfonamide

: 1178907-41-9
N-(6-(2-hydroxybut-3-en-2-yl)benzo[d][1,3]dioxol-5-yl)-4-methylbenzenesulfonamide

Guidance literature:: N-(6-acetylbenzo[d][1,3]dioxol-5-yl)-4-methylbenzenesulfonamide; With pyridine; toluene-4-sulfonic acid; at 20 ℃; for 4h;

vinyl magnesium bromide; In tetrahydrofuran; for 3h; Reflux;

With ammonium chloride; In tetrahydrofuran; at 20 ℃; for 0.166667h;
DOI:10.1021/jo900917q

Reference yield: 45.0%

: 1178907-41-9
N-(6-(2-hydroxybut-3-en-2-yl)benzo[d][1,3]dioxol-5-yl)-4-methylbenzenesulfonamide

: 1178907-54-4
8-methyl-5-tosyl-5,6-dihydro-[1,3]dioxolo[4,5-g]quinoline

Guidance literature:: With gold(III) chloride; silver hexafluoroantimonate; In toluene; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/jo900917q