phenyl(2-trifluoracetamido-2-deoxy-3,4,6-tri-O-acetyl-1-thio-D-glucopyranoside)

Base Information

Chemical Name:phenyl(2-trifluoracetamido-2-deoxy-3,4,6-tri-O-acetyl-1-thio-D-glucopyranoside)
CAS No.:225242-73-9
Molecular Formula:C₂₀H₂₂F₃NO₈S
Molecular Weight:493.458
Hs Code.:

Synonyms:phenyl(2-trifluoracetamido-2-deoxy-3,4,6-tri-O-acetyl-1-thio-D-glucopyranoside)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of phenyl(2-trifluoracetamido-2-deoxy-3,4,6-tri-O-acetyl-1-thio-D-glucopyranoside)

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Technology Process of phenyl(2-trifluoracetamido-2-deoxy-3,4,6-tri-O-acetyl-1-thio-D-glucopyranoside)

There total 6 articles about phenyl(2-trifluoracetamido-2-deoxy-3,4,6-tri-O-acetyl-1-thio-D-glucopyranoside) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 7139-63-1
1,3,4,6-tetra-O-acetyl-2-(trifluoroacetamido)-2-deoxy-β-D-glucopyranoside

: 108-98-5
thiophenol

: 225242-73-9
phenyl(2-trifluoracetamido-2-deoxy-3,4,6-tri-O-acetyl-1-thio-D-glucopyranoside)

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane;
DOI:10.1021/jo9903499

Reference yield: 75.0%

: 108-98-5
thiophenol

: 137766-83-7
2-deoxy-2-trifluoroacetamido-1,3,4,6-tetra-O-acetyl-α,β-D-glucopyranoside

: 225242-73-9
phenyl(2-trifluoracetamido-2-deoxy-3,4,6-tri-O-acetyl-1-thio-D-glucopyranoside)

Guidance literature:: With boron trifluoride diethyl etherate;
DOI:10.1016/j.tetasy.2009.05.007

Reference yield:

: 7597-81-1
1,3,4,6-tetra-O-acetyl-2-deoxy-2-(4-methoxybenzylidene)amino-β-D-glucopyranose

: 225242-73-9
phenyl(2-trifluoracetamido-2-deoxy-3,4,6-tri-O-acetyl-1-thio-D-glucopyranoside)

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / HCl / acetone

2: 100 percent / pyridine / CH₂Cl₂

3: 92 percent / BF₃*OEt₂ / CH₂Cl₂

With pyridine; hydrogenchloride; boron trifluoride diethyl etherate; In dichloromethane; acetone; 1: Hydrolysis / 2: Acylation / 3: Substitution;
DOI:10.1021/jo9903499