2-deoxy-2-trifluoroacetamido-1,3,4,6-tetra-O-acetyl-α,β-D-glucopyranoside

Base Information

• Chemical Name: 2-deoxy-2-trifluoroacetamido-1,3,4,6-tetra-O-acetyl-α,β-D-glucopyranoside
• CAS No.: 137766-83-7
• Molecular Formula: C₁₆H₂₀F₃NO₁₀
• Molecular Weight: 443.331

Synonyms:2-deoxy-2-trifluoroacetamido-1,3,4,6-tetra-O-acetyl-α,β-D-glucopyranoside

Chemical Property of 2-deoxy-2-trifluoroacetamido-1,3,4,6-tetra-O-acetyl-α,β-D-glucopyranoside

Chemical Property:

Purity/Quality:

95% ^*data from raw suppliers

Ac4GlcNAcF3 ^*data from reagent suppliers

Safty Information:

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Technology Process of 2-deoxy-2-trifluoroacetamido-1,3,4,6-tetra-O-acetyl-α,β-D-glucopyranoside

There total 1 articles about 2-deoxy-2-trifluoroacetamido-1,3,4,6-tetra-O-acetyl-α,β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 1,3,4,6-Tetra-O-acetyl-2-desoxy-2-trifluoracetamino-D-glucose (7139-63-1,25258-08-6,25258-09-7,25258-10-0,86900-32-5,137766-83-7)

Guidance literature:

1,3,4,6-Tetra-O-acetyl-2-amino-2-desoxy-β-D-glucose, Trifluoracetanhydrid in Pyridin;

DOI:10.1039/C1966000146a

Reference yield: 84.0%

para-thiocresol (106-45-6) + 2-deoxy-2-trifluoroacetamido-1,3,4,6-tetra-O-acetyl-α,β-D-glucopyranoside (137766-83-7) → p-tolyl 3,4,6-tri-O-acetyl-2-trifluoroacetamido-2-deoxy-β-1-thio-D-glucopyranoside

Guidance literature:

With boron trifluoride diethyl etherate; In dichloromethane; at 20 ℃; for 40h; Inert atmosphere;

DOI:10.1039/c9ob02079a

Reference yield: 75.0%

thiophenol (108-98-5) + 2-deoxy-2-trifluoroacetamido-1,3,4,6-tetra-O-acetyl-α,β-D-glucopyranoside (137766-83-7) → phenyl(2-trifluoracetamido-2-deoxy-3,4,6-tri-O-acetyl-1-thio-D-glucopyranoside) (225242-73-9)

Guidance literature:

With boron trifluoride diethyl etherate;

DOI:10.1016/j.tetasy.2009.05.007

Downstream raw materials:

uridine 5'-(2-amino-2-deoxy-α-D-glucopyranosyl)-diphosphate

3,4,6-tri-O-acetyl-2-deoxy-2-trifluoroacetylamino-α-D-glucopyranosyl dibenzyl phosphate

Acetic acid (2R,3S,4R,5R,6S)-3-acetoxy-2-acetoxymethyl-6-(bis-benzyloxy-phosphoryloxy)-5-(2,2,2-trifluoro-acetylamino)-tetrahydro-pyran-4-yl ester

phenyl(2-trifluoracetamido-2-deoxy-3,4,6-tri-O-acetyl-1-thio-D-glucopyranoside)

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