C₄₄H₅₄O₆Si

Base Information

Chemical Name:C₄₄H₅₄O₆Si
CAS No.:950190-99-5
Molecular Formula:C₄₄H₅₄O₆Si
Molecular Weight:706.995
Hs Code.:

C<sub>44</sub>H<sub>54</sub>O<sub>6</sub>Si

Synonyms:C₄₄H₅₄O₆Si

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Chemical Property of C₄₄H₅₄O₆Si

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Technology Process of C₄₄H₅₄O₆Si

There total 8 articles about C₄₄H₅₄O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 950190-98-4
C₃₇H₄₈O₆Si

: 100-39-0
benzyl bromide

: 950190-99-5
C₄₄H₅₄O₆Si

Guidance literature:: With tetra-(n-butyl)ammonium iodide; sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 4h;
DOI:10.1021/ol071282b

Reference yield:

: 950190-84-8
C₃₆H₆₂O₆S₄Si

: 950190-99-5
C₄₄H₅₄O₆Si

Guidance literature:: Multi-step reaction with 6 steps

1: 75 percent / calcium carbonate; mercury(II) perchlorate trihydrate / tetrahydrofuran; H₂O / 0.08 h / 0 °C

2: tetramethylammonium triacetoxyborohydride; acetic acid / acetonitrile / 96 h / -35 °C

3: p-toluenesulfonic acid monohydrate / acetone / 0.13 h / 20 °C

4: 2.0 g / perchloric acid / CH₂Cl₂; H₂O / 36 h / 20 °C

5: 84 percent / imidazole; 4-dimethylaminopyridine / CH₂Cl₂ / 0.5 h / 0 °C

6: 97 percent / sodium hydride; tetrabutylammonium iodide / dimethylformamide; various solvent(s) / 4 h / 20 °C

With 1H-imidazole; dmap; perchloric acid; mercury(II) perchlorate; tetra-(n-butyl)ammonium iodide; sodium hydride; toluene-4-sulfonic acid; acetic acid; calcium carbonate; tetramethylammonium triacetoxyborohydride; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1021/ol071282b

Reference yield:

: 950190-83-7
C₁₃H₂₄O₃S₂

: 950190-99-5
C₄₄H₅₄O₆Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: potassium tert-butoxide; n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C

1.2: tetrahydrofuran; hexane / 2 h / -78 °C

1.3: 77 percent / tetrahydrofuran; hexane / 0.83 h / -78 - 0 °C

2.1: 75 percent / calcium carbonate; mercury(II) perchlorate trihydrate / tetrahydrofuran; H₂O / 0.08 h / 0 °C

3.1: tetramethylammonium triacetoxyborohydride; acetic acid / acetonitrile / 96 h / -35 °C

4.1: p-toluenesulfonic acid monohydrate / acetone / 0.13 h / 20 °C

5.1: 2.0 g / perchloric acid / CH₂Cl₂; H₂O / 36 h / 20 °C

6.1: 84 percent / imidazole; 4-dimethylaminopyridine / CH₂Cl₂ / 0.5 h / 0 °C

7.1: 97 percent / sodium hydride; tetrabutylammonium iodide / dimethylformamide; various solvent(s) / 4 h / 20 °C

With 1H-imidazole; dmap; n-butyllithium; perchloric acid; mercury(II) perchlorate; potassium tert-butylate; tetra-(n-butyl)ammonium iodide; sodium hydride; toluene-4-sulfonic acid; acetic acid; calcium carbonate; tetramethylammonium triacetoxyborohydride; In tetrahydrofuran; hexane; dichloromethane; water; N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1021/ol071282b