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C60H50O16

Base Information
  • Chemical Name:C60H50O16
  • CAS No.:847237-53-0
  • Molecular Formula:C60H50O16
  • Molecular Weight:1027.05
  • Hs Code.:
C<sub>60</sub>H<sub>50</sub>O<sub>16</sub>

Synonyms:C60H50O16

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Chemical Property of C60H50O16
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Technology Process of C60H50O16

There total 8 articles about C60H50O16 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; at 80 ℃; for 1h;
DOI:10.1016/j.carres.2004.11.017
Guidance literature:
Multi-step reaction with 8 steps
1: 83 percent / molecular sieves 4 Angstroem; boron trifluoride etherate / CH2Cl2
2: 9.8 g / NaOMe / methanol / 20 °C
3: 3.0 g / H2SO4 / dimethylformamide; acetone / 1 h / Heating
4: 5.86 g / pyridine / 3 h / 20 °C
5: 89 percent / acetic acid; H2O / 1 h / 95 °C
6: 60 percent / pyridine / 3 h / 20 °C
7: 4-(N,N-dimethylamino)pyridine / CH2Cl2 / 20 °C
8: 0.41 g / tributyltin hydride; azoisobutyronitrile / benzene / 1 h / 80 °C
With dmap; 2,2'-azobis(isobutyronitrile); 4 A molecular sieve; sulfuric acid; boron trifluoride diethyl etherate; tri-n-butyl-tin hydride; sodium methylate; In pyridine; methanol; dichloromethane; water; acetic acid; N,N-dimethyl-formamide; acetone; benzene;
DOI:10.1016/j.carres.2004.11.017
Guidance literature:
Multi-step reaction with 7 steps
1: 9.8 g / NaOMe / methanol / 20 °C
2: 3.0 g / H2SO4 / dimethylformamide; acetone / 1 h / Heating
3: 5.86 g / pyridine / 3 h / 20 °C
4: 89 percent / acetic acid; H2O / 1 h / 95 °C
5: 60 percent / pyridine / 3 h / 20 °C
6: 4-(N,N-dimethylamino)pyridine / CH2Cl2 / 20 °C
7: 0.41 g / tributyltin hydride; azoisobutyronitrile / benzene / 1 h / 80 °C
With dmap; 2,2'-azobis(isobutyronitrile); sulfuric acid; tri-n-butyl-tin hydride; sodium methylate; In pyridine; methanol; dichloromethane; water; acetic acid; N,N-dimethyl-formamide; acetone; benzene;
DOI:10.1016/j.carres.2004.11.017
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