(S)-1-((4S,5R)-5-(1,3-dithian-2-yl)-2,2-dimethyl-1,3-dioxolan-4-yl)propan-2-yl benzoate

Base Information

Chemical Name:(S)-1-((4S,5R)-5-(1,3-dithian-2-yl)-2,2-dimethyl-1,3-dioxolan-4-yl)propan-2-yl benzoate
CAS No.:86040-00-8
Molecular Formula:C₁₉H₂₆O₄S₂
Molecular Weight:382.545
Hs Code.:

Synonyms:(S)-1-((4S,5R)-5-(1,3-dithian-2-yl)-2,2-dimethyl-1,3-dioxolan-4-yl)propan-2-yl benzoate

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Chemical Property of (S)-1-((4S,5R)-5-(1,3-dithian-2-yl)-2,2-dimethyl-1,3-dioxolan-4-yl)propan-2-yl benzoate

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Technology Process of (S)-1-((4S,5R)-5-(1,3-dithian-2-yl)-2,2-dimethyl-1,3-dioxolan-4-yl)propan-2-yl benzoate

There total 7 articles about (S)-1-((4S,5R)-5-(1,3-dithian-2-yl)-2,2-dimethyl-1,3-dioxolan-4-yl)propan-2-yl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 76331-10-7
(R)-1-((4S,5R)-5-(1,3-dithian-2-yl)-2,2-dimethyl-1,3-dioxolan-4-yl)propan-2-ol

: 65-85-0,8013-63-6
benzoic acid

: 86040-00-8
(S)-1-((4S,5R)-5-(1,3-dithian-2-yl)-2,2-dimethyl-1,3-dioxolan-4-yl)propan-2-yl benzoate

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; for 0.5h; Ambient temperature;

Reference yield:

: 20585-18-6
methyl 4,6-dideoxy-α-D-glucopyranoside

: 86040-00-8
(S)-1-((4S,5R)-5-(1,3-dithian-2-yl)-2,2-dimethyl-1,3-dioxolan-4-yl)propan-2-yl benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / aq. HCl / 12 h

2: 95 percent / CuSO₄; H₂SO₄ / 12 h

3: 82 percent / Ph₃P; diethyl azodicarboxylate / tetrahydrofuran / 1 h

With hydrogenchloride; sulfuric acid; copper(II) sulfate; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; 3: Mitsunobu reaction;
DOI:10.1039/b505980a

Reference yield:

: 76331-09-4
4,6-Didesoxy-D-xylo-hexose-trimethylendithioacetal

: 86040-00-8
(S)-1-((4S,5R)-5-(1,3-dithian-2-yl)-2,2-dimethyl-1,3-dioxolan-4-yl)propan-2-yl benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / CuSO₄; H₂SO₄ / 12 h

2: 82 percent / Ph₃P; diethyl azodicarboxylate / tetrahydrofuran / 1 h

With sulfuric acid; copper(II) sulfate; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; 2: Mitsunobu reaction;
DOI:10.1039/b505980a