2-(4-Methylnaphthalen-1-yl)-4-nitrobenzoic acid

Base Information

Chemical Name:2-(4-Methylnaphthalen-1-yl)-4-nitrobenzoic acid
CAS No.:180977-37-1
Molecular Formula:C₁₇H₁₁NO₄
Molecular Weight:293.279
Hs Code.:
DSSTox Substance ID:DTXSID10695522
Wikidata:Q82624741

Synonyms:DTXSID10695522;2-(4-methylnaphthalen-1-yl)-4-nitrobenzoic acid

Suppliers and Price of 2-(4-Methylnaphthalen-1-yl)-4-nitrobenzoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 2-(4-Methylnaphthalen-1-yl)-4-nitrobenzoic acid

Chemical Property:

XLogP3:4.5
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:307.08445790
Heavy Atom Count:23
Complexity:460

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C2=CC=CC=C12)C3=C(C=CC(=C3)[N+](=O)[O-])C(=O)O

Technology Process of 2-(4-Methylnaphthalen-1-yl)-4-nitrobenzoic acid

There total 5 articles about 2-(4-Methylnaphthalen-1-yl)-4-nitrobenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 180977-38-2
4-nitro-2-(1-naphthyl)benzoic acid methyl ester

: 180977-37-1
4-nitro-2-(1-naphthyl)benzoic acid

Guidance literature:: With sodium hydroxide; In methanol; for 2h; Heating;
DOI:10.1016/S0968-0896(99)00252-7

Reference yield:

: 100959-22-6
methyl 2-bromo-4-nitrobenzoate

: 180977-37-1
4-nitro-2-(1-naphthyl)benzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / Na₃PO₄; Pd(PPh₃)4 / dimethylformamide / 100 °C

2: 98 percent / aq. NaOH / methanol / 2 h / Heating

With sodium hydroxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium phosphate; In methanol; N,N-dimethyl-formamide; 1: Substitution / 2: Hydrolysis;
DOI:10.1016/S0968-0896(99)00252-7

Reference yield:

: 13922-41-3
1-Naphthylboronic acid

: 180977-37-1
4-nitro-2-(1-naphthyl)benzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 73 percent / Na₃PO₄; Pd(PPh₃)4 / dimethylformamide / 100 °C

2: 98 percent / aq. NaOH / methanol / 2 h / Heating

With sodium hydroxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium phosphate; In methanol; N,N-dimethyl-formamide; 1: Substitution / 2: Hydrolysis;
DOI:10.1016/S0968-0896(99)00252-7