N-acetyl-α-D-muramic acid, 4,6-diacetate, 1-(benzyl hexadecyl phosphate)

Base Information

Chemical Name:N-acetyl-α-D-muramic acid, 4,6-diacetate, 1-(benzyl hexadecyl phosphate)
CAS No.:1380522-15-5
Molecular Formula:C₃₈H₆₂NO₁₃P
Molecular Weight:771.883
Hs Code.:

Synonyms:N-acetyl-α-D-muramic acid, 4,6-diacetate, 1-(benzyl hexadecyl phosphate)

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Chemical Property of N-acetyl-α-D-muramic acid, 4,6-diacetate, 1-(benzyl hexadecyl phosphate)

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Technology Process of N-acetyl-α-D-muramic acid, 4,6-diacetate, 1-(benzyl hexadecyl phosphate)

There total 10 articles about N-acetyl-α-D-muramic acid, 4,6-diacetate, 1-(benzyl hexadecyl phosphate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1380522-09-7
C₄₆H₇₀NO₁₅PS

: 1380522-15-5
N-acetyl-α-D-muramic acid, 4,6-diacetate, 1-(benzyl hexadecyl phosphate)

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 0 - 20 ℃; for 1.5h;
DOI:10.1021/ja302099u

Reference yield:

: C₄₆H₇₀NO₁₄PS

: 1380522-15-5
N-acetyl-α-D-muramic acid, 4,6-diacetate, 1-(benzyl hexadecyl phosphate)

Guidance literature:: Multi-step reaction with 2 steps

1: dihydrogen peroxide / water; acetonitrile / 0.58 h / -78 - 20 °C

2: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 1.5 h / 0 - 20 °C

With dihydrogen peroxide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; water; acetonitrile;
DOI:10.1021/ja302099u

Reference yield:

: 7512-17-6,72-87-7,1136-42-1,1136-44-3,6082-29-7,6730-06-9,7772-94-3,10036-64-3,14131-60-3,14131-64-7,14131-68-1,14215-68-0,62057-49-2,62057-50-5,62057-51-6,62057-52-7,62057-53-8,62057-54-9,62057-55-0,62057-56-1,62075-50-7,62137-54-6,134451-97-1,134522-12-6,148347-16-4
N-Acetyl-D-glucosamine

: 1380522-15-5
N-acetyl-α-D-muramic acid, 4,6-diacetate, 1-(benzyl hexadecyl phosphate)

Guidance literature:: Multi-step reaction with 10 steps

1: toluene-4-sulfonic acid / toluene / 3 h / Reflux

2: toluene-4-sulfonic acid; orthoformic acid triethyl ester / 1,4-dioxane; N,N-dimethyl-formamide / 3 h / 20 °C / 97.51 - 120.01 Torr

3: sodium hydride / 1,4-dioxane / 65 °C

4: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 8 h / 0 - 20 °C

5: acetic acid / water / 2 h / 60 °C

6: pyridine / 3 h / 20 °C

7: palladium 10% on activated carbon; hydrogen / methanol / 5 h / 760.05 Torr

8: 1H-tetrazole / acetonitrile / 8 h / 20 °C

9: dihydrogen peroxide / water; acetonitrile / 0.58 h / -78 - 20 °C

10: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 1.5 h / 0 - 20 °C

With 1H-tetrazole; dmap; palladium 10% on activated carbon; hydrogen; dihydrogen peroxide; sodium hydride; toluene-4-sulfonic acid; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; orthoformic acid triethyl ester; In 1,4-dioxane; pyridine; methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile;
DOI:10.1021/ja302099u