(5Z,8R,9E)-8-[1-(tert-butyl)-1,1-diphenylsilyl]oxy-10-iodo-5,9-decadienoic acid

Base Information

Chemical Name:(5Z,8R,9E)-8-[1-(tert-butyl)-1,1-diphenylsilyl]oxy-10-iodo-5,9-decadienoic acid
CAS No.:1252798-63-2
Molecular Formula:C₂₆H₃₃IO₃Si
Molecular Weight:548.536
Hs Code.:

Synonyms:(5Z,8R,9E)-8-[1-(tert-butyl)-1,1-diphenylsilyl]oxy-10-iodo-5,9-decadienoic acid

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Chemical Property of (5Z,8R,9E)-8-[1-(tert-butyl)-1,1-diphenylsilyl]oxy-10-iodo-5,9-decadienoic acid

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Technology Process of (5Z,8R,9E)-8-[1-(tert-butyl)-1,1-diphenylsilyl]oxy-10-iodo-5,9-decadienoic acid

There total 1 articles about (5Z,8R,9E)-8-[1-(tert-butyl)-1,1-diphenylsilyl]oxy-10-iodo-5,9-decadienoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1252798-85-8
methyl (5Z,8R,9E)-8-[1-(tert-butyl)-1,1-diphenylsilyl]oxy-10-iodo-5,9-decadienoate

: 1252798-63-2
(5Z,8R,9E)-8-[1-(tert-butyl)-1,1-diphenylsilyl]oxy-10-iodo-5,9-decadienoic acid

Guidance literature:: With water; lithium hydroxide; In tetrahydrofuran; at 20 ℃; for 6h; Inert atmosphere;
DOI:10.1002/ejoc.201000565

Reference yield: 87.0%

: 1252798-64-3
(2R,4Z,7Z)-1-[(4-methoxybenzyl)oxy]-4,7-decadien-2-ol

: 1252798-63-2
(5Z,8R,9E)-8-[1-(tert-butyl)-1,1-diphenylsilyl]oxy-10-iodo-5,9-decadienoic acid

: 1252798-61-0
(1R,3Z,6Z)-1-{[(4-methoxybenzyl)oxy]methyl}nona-3,6-dien-1-yl (5Z,8R,9E)-8-{[tert-butyl(diphenyl)silyl]oxy}-10-iododeca-5,9-dienoate

Guidance literature:: (5Z,8R,9E)-8-[1-(tert-butyl)-1,1-diphenylsilyl]oxy-10-iodo-5,9-decadienoic acid; With 2,4,6-trichlorobenzoyl chloride; triethylamine; In tetrahydrofuran; at 0 ℃; for 0.5h; Inert atmosphere;

(2R,4Z,7Z)-1-[(4-methoxybenzyl)oxy]-4,7-decadien-2-ol; With dmap; In benzene; at 0 - 20 ℃; for 6h; Inert atmosphere;
DOI:10.1002/ejoc.201000565