methyl 4-<(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphalenyl)carboxamido>benzoate

Base Information

Chemical Name:methyl 4-<(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphalenyl)carboxamido>benzoate
CAS No.:102121-59-5
Molecular Formula:C₂₃H₂₇NO₃
Molecular Weight:365.472
Hs Code.:

Synonyms:methyl 4-<(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphalenyl)carboxamido>benzoate

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Chemical Property of methyl 4-<(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphalenyl)carboxamido>benzoate

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Technology Process of methyl 4-<(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphalenyl)carboxamido>benzoate

There total 2 articles about methyl 4-<(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphalenyl)carboxamido>benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 104224-50-2
5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphtholyl chloride

: 619-45-4
4-methoxycarbonyl aniline

: 102121-59-5
methyl 4-<(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphalenyl)carboxamido>benzoate

Guidance literature:: DOI:10.1248/cpb.34.2275

Reference yield:

: 103031-30-7
5,6,7,8-tetrahydro-5,5,8,8-tetramethylnaphthalene-2-carboxylic acid

: 619-45-4
4-methoxycarbonyl aniline

: 102121-59-5
methyl 4-<(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphalenyl)carboxamido>benzoate

Guidance literature:: With dmap; thionyl chloride; Yield given. Multistep reaction; 1.) 0 deg C, 30 min, 2.) pyridine, 60 deg C, 2 h;
DOI:10.1021/jm00119a021

Reference yield: 78.0%

: 102121-59-5
methyl 4-<(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphalenyl)carboxamido>benzoate

: 102121-60-8
Am580

Guidance literature:: methyl 4-<(5,6,7,8-tetrahydro-5,5,8,8-tetramethyl-2-naphalenyl)carboxamido>benzoate; With methanol; potassium hydroxide; for 16h; Heating / reflux;

With hydrogenchloride; In water; ethyl acetate;