1,3,2',6'-tetrakis(n-benzyloxycarbonyl)-5,6-O-cyclohexyl-3',4'-di-O-methoxymethylneamine

Base Information

Chemical Name:1,3,2',6'-tetrakis(n-benzyloxycarbonyl)-5,6-O-cyclohexyl-3',4'-di-O-methoxymethylneamine
CAS No.:419573-38-9
Molecular Formula:C₅₄H₆₆N₄O₁₆
Molecular Weight:1027.14
Hs Code.:

Synonyms:1,3,2',6'-tetrakis(n-benzyloxycarbonyl)-5,6-O-cyclohexyl-3',4'-di-O-methoxymethylneamine

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Chemical Property of 1,3,2',6'-tetrakis(n-benzyloxycarbonyl)-5,6-O-cyclohexyl-3',4'-di-O-methoxymethylneamine

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Technology Process of 1,3,2',6'-tetrakis(n-benzyloxycarbonyl)-5,6-O-cyclohexyl-3',4'-di-O-methoxymethylneamine

There total 5 articles about 1,3,2',6'-tetrakis(n-benzyloxycarbonyl)-5,6-O-cyclohexyl-3',4'-di-O-methoxymethylneamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 55728-75-1
1,3,2',6'-tetrakis(N-benzyloxycarbonyl)-5,6-O-cyclohexylideneneamine

: 107-30-2
chloromethyl methyl ether

: 419573-38-9
1,3,2',6'-tetrakis(n-benzyloxycarbonyl)-5,6-O-cyclohexyl-3',4'-di-O-methoxymethylneamine

Guidance literature:: With tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 32 ℃; for 40h;
DOI:10.1021/ja011695m

Reference yield:

: 22854-75-7
N,N',N'',N'''-tetra(benzyloxycarbonyl)neamine

: 419573-38-9
1,3,2',6'-tetrakis(n-benzyloxycarbonyl)-5,6-O-cyclohexyl-3',4'-di-O-methoxymethylneamine

Guidance literature:: Multi-step reaction with 2 steps

1: 56.6 percent / TsOH / dimethylformamide / 36 h / 20 °C

2: 79 percent / Bu₄NI; (i-Pr)2NEt / dimethylformamide / 40 h / 32 °C

With tetra-(n-butyl)ammonium iodide; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide;
DOI:10.1021/ja011695m

Reference yield:

: 3947-65-7
neomycin A

: 419573-38-9
1,3,2',6'-tetrakis(n-benzyloxycarbonyl)-5,6-O-cyclohexyl-3',4'-di-O-methoxymethylneamine

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / aq. Na₂CO₃ / acetone

2: 56.6 percent / TsOH / dimethylformamide / 36 h / 20 °C

3: 79 percent / Bu₄NI; (i-Pr)2NEt / dimethylformamide / 40 h / 32 °C

With tetra-(n-butyl)ammonium iodide; sodium carbonate; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; acetone;
DOI:10.1021/ja011695m