Technology Process of C18H27N3O5S
There total 1 articles about C18H27N3O5S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate / acetonitrile / Reflux
2: triethylamine / dichloromethane / 15 - 20 °C
3: caesium carbonate / acetonitrile / 60 °C
With
potassium carbonate; caesium carbonate; triethylamine;
In
dichloromethane; acetonitrile;
- Guidance literature:
-
With
hydrogen;
5%-palladium/activated carbon;
In
tetrahydrofuran;
at 20 ℃;
for 16h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: hydrogen / 5%-palladium/activated carbon / tetrahydrofuran / 16 h / 20 °C
2: hydrogen bromide / 8 h / 150 °C
3: triethylamine / N,N-dimethyl-formamide / 20 °C
4: tetrahydrofuran / 3 h / 20 °C
5: dihydrogen peroxide; acetic acid / water / 3 h / 20 °C
With
hydrogen bromide; hydrogen; dihydrogen peroxide; acetic acid; triethylamine;
5%-palladium/activated carbon;
In
tetrahydrofuran; water; N,N-dimethyl-formamide;