4-amino-2-{(2E)-2-[1-(2-bromo-5-chlorophenyl)-4,4,5.5,5-pentarluoropentylidene]hydrazinyl}-5-methyl-5-phenyl-5,7-dihydro-6H-pyrrolo[2,3-d]pyrimidin-6-one

Base Information

Chemical Name:4-amino-2-{(2E)-2-[1-(2-bromo-5-chlorophenyl)-4,4,5.5,5-pentarluoropentylidene]hydrazinyl}-5-methyl-5-phenyl-5,7-dihydro-6H-pyrrolo[2,3-d]pyrimidin-6-one
CAS No.:1350855-84-3
Molecular Formula:C₂₄H₁₉BrClF₅N₆O
Molecular Weight:617.803
Hs Code.:

4-amino-2-{(2E)-2-[1-(2-bromo-5-chlorophenyl)-4,4,5.5,5-pentarluoropentylidene]hydrazinyl}-5-methyl-5-phenyl-5,7-dihydro-6H-pyrrolo[2,3-d]pyrimidin-6-one

Synonyms:4-amino-2-{(2E)-2-[1-(2-bromo-5-chlorophenyl)-4,4,5.5,5-pentarluoropentylidene]hydrazinyl}-5-methyl-5-phenyl-5,7-dihydro-6H-pyrrolo[2,3-d]pyrimidin-6-one

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Chemical Property of 4-amino-2-{(2E)-2-[1-(2-bromo-5-chlorophenyl)-4,4,5.5,5-pentarluoropentylidene]hydrazinyl}-5-methyl-5-phenyl-5,7-dihydro-6H-pyrrolo[2,3-d]pyrimidin-6-one

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Technology Process of 4-amino-2-{(2E)-2-[1-(2-bromo-5-chlorophenyl)-4,4,5.5,5-pentarluoropentylidene]hydrazinyl}-5-methyl-5-phenyl-5,7-dihydro-6H-pyrrolo[2,3-d]pyrimidin-6-one

There total 3 articles about 4-amino-2-{(2E)-2-[1-(2-bromo-5-chlorophenyl)-4,4,5.5,5-pentarluoropentylidene]hydrazinyl}-5-methyl-5-phenyl-5,7-dihydro-6H-pyrrolo[2,3-d]pyrimidin-6-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 148043-73-6
4,4,5,5,5-pentafluorpentan-1-ol

: 1350855-84-3
4-amino-2-{(2E)-2-[1-(2-bromo-5-chlorophenyl)-4,4,5.5,5-pentarluoropentylidene]hydrazinyl}-5-methyl-5-phenyl-5,7-dihydro-6H-pyrrolo[2,3-d]pyrimidin-6-one

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium permanganate monohydrate / tetraethylammonium hydrogen sulphate / water / 4.33 h / 70 °C / Inert atmosphere

1.2: pH 1

2.1: sodium hexamethyldisilazane / tetrahydrofuran / -78 - 0 °C / Inert atmosphere

3.1: boron trifluoride diethyl etherate / methanol / 3 h / 100 °C / Inert atmosphere

4.1: sodium hydrogencarbonate / methanol / 0.67 h / 135 °C / Inert atmosphere; microwave irradiation

With sodium permanganate monohydrate; boron trifluoride diethyl etherate; sodium hexamethyldisilazane; sodium hydrogencarbonate; tetraethylammonium hydrogen sulphate; In tetrahydrofuran; methanol; water;

Reference yield:

: 3637-31-8
4,4,5,5,5-pentafluoropentanoic acid

: 1350855-84-3
4-amino-2-{(2E)-2-[1-(2-bromo-5-chlorophenyl)-4,4,5.5,5-pentarluoropentylidene]hydrazinyl}-5-methyl-5-phenyl-5,7-dihydro-6H-pyrrolo[2,3-d]pyrimidin-6-one

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hexamethyldisilazane / tetrahydrofuran / -78 - 0 °C / Inert atmosphere

2: boron trifluoride diethyl etherate / methanol / 3 h / 100 °C / Inert atmosphere

3: sodium hydrogencarbonate / methanol / 0.67 h / 135 °C / Inert atmosphere; microwave irradiation

With boron trifluoride diethyl etherate; sodium hexamethyldisilazane; sodium hydrogencarbonate; In tetrahydrofuran; methanol;

Reference yield:

: 1350855-82-1
1-(2-bromo-5-chlorophenyl)-4,4,5,5,5-pentafluoropentan-1-one

: 1350855-84-3
4-amino-2-{(2E)-2-[1-(2-bromo-5-chlorophenyl)-4,4,5.5,5-pentarluoropentylidene]hydrazinyl}-5-methyl-5-phenyl-5,7-dihydro-6H-pyrrolo[2,3-d]pyrimidin-6-one

Guidance literature:: Multi-step reaction with 2 steps

1: boron trifluoride diethyl etherate / methanol / 3 h / 100 °C / Inert atmosphere

2: sodium hydrogencarbonate / methanol / 0.67 h / 135 °C / Inert atmosphere; microwave irradiation

With boron trifluoride diethyl etherate; sodium hydrogencarbonate; In methanol;