1-((((1S,3R)-3-(2-bromoethoxy)-4-iodo-1-phenylbutoxy)methyl)sulfonyl)-4-methylbenzene

Base Information

Chemical Name:1-((((1S,3R)-3-(2-bromoethoxy)-4-iodo-1-phenylbutoxy)methyl)sulfonyl)-4-methylbenzene
CAS No.:1449417-68-8
Molecular Formula:C₂₀H₂₄BrIO₄S
Molecular Weight:567.283
Hs Code.:

Synonyms:1-((((1S,3R)-3-(2-bromoethoxy)-4-iodo-1-phenylbutoxy)methyl)sulfonyl)-4-methylbenzene

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Chemical Property of 1-((((1S,3R)-3-(2-bromoethoxy)-4-iodo-1-phenylbutoxy)methyl)sulfonyl)-4-methylbenzene

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Technology Process of 1-((((1S,3R)-3-(2-bromoethoxy)-4-iodo-1-phenylbutoxy)methyl)sulfonyl)-4-methylbenzene

There total 4 articles about 1-((((1S,3R)-3-(2-bromoethoxy)-4-iodo-1-phenylbutoxy)methyl)sulfonyl)-4-methylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 1538-98-3
p-tosyldiazomethane

: 1449417-64-4
(1S,3R)-3-(2-bromoethoxy)-4-iodo-1-phenylbutan-1-ol

: 1449417-68-8
1-((((1S,3R)-3-(2-bromoethoxy)-4-iodo-1-phenylbutoxy)methyl)sulfonyl)-4-methylbenzene

Guidance literature:: With tetrafluoroboric acid diethyl ether; In dichloromethane; at 0 ℃; for 2h; Inert atmosphere;
DOI:10.1016/j.tet.2013.05.081

Reference yield:

: 1449417-62-2
(S)-(1-((2-bromoethoxy)methoxy)but-3-en-1-yl)benzene

: 1449417-68-8
1-((((1S,3R)-3-(2-bromoethoxy)-4-iodo-1-phenylbutoxy)methyl)sulfonyl)-4-methylbenzene

Guidance literature:: Multi-step reaction with 3 steps

1: N-iodo-succinimide / nitromethane / 6 h / 2 °C / Darkness; Inert atmosphere

2: 3-chloro-benzenecarboperoxoic acid; sodium hydrogencarbonate / ethyl acetate / 1 h / 20 °C

3: tetrafluoroboric acid diethyl ether / dichloromethane / 2 h / 0 °C / Inert atmosphere

With tetrafluoroboric acid diethyl ether; N-iodo-succinimide; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In nitromethane; dichloromethane; ethyl acetate;
DOI:10.1016/j.tet.2013.05.081

Reference yield:

: 1449418-05-6
C₂₀H₂₂BrIN₄O₂S

: 1449417-68-8
1-((((1S,3R)-3-(2-bromoethoxy)-4-iodo-1-phenylbutoxy)methyl)sulfonyl)-4-methylbenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 3-chloro-benzenecarboperoxoic acid; sodium hydrogencarbonate / ethyl acetate / 1 h / 20 °C

2: tetrafluoroboric acid diethyl ether / dichloromethane / 2 h / 0 °C / Inert atmosphere

With tetrafluoroboric acid diethyl ether; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; ethyl acetate;
DOI:10.1016/j.tet.2013.05.081