(E)-ethyl 4-(benzylideneamino)-3-(2-(N,4-dimethylphenylsulfonamido)-2-oxoethyl)benzoate

Base Information

Chemical Name:(E)-ethyl 4-(benzylideneamino)-3-(2-(N,4-dimethylphenylsulfonamido)-2-oxoethyl)benzoate
CAS No.:1403981-67-8
Molecular Formula:C₂₆H₂₆N₂O₅S
Molecular Weight:478.569
Hs Code.:

Synonyms:(E)-ethyl 4-(benzylideneamino)-3-(2-(N,4-dimethylphenylsulfonamido)-2-oxoethyl)benzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-ethyl 4-(benzylideneamino)-3-(2-(N,4-dimethylphenylsulfonamido)-2-oxoethyl)benzoate

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Technology Process of (E)-ethyl 4-(benzylideneamino)-3-(2-(N,4-dimethylphenylsulfonamido)-2-oxoethyl)benzoate

There total 1 articles about (E)-ethyl 4-(benzylideneamino)-3-(2-(N,4-dimethylphenylsulfonamido)-2-oxoethyl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1005500-75-3
N-(methyl)-N-(p-toluenesulfonyl)ethynylamine

: 94664-79-6,51911-71-8
N-(4-carboethoxyphenyl)-α-phenylnitrone

: 1403981-67-8
(E)-ethyl 4-(benzylideneamino)-3-(2-(N,4-dimethylphenylsulfonamido)-2-oxoethyl)benzoate

Guidance literature:: With platinum(II) chloride; In 1,2-dichloro-ethane; at 28 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/ol302621z

Reference yield:

: 1403981-67-8
(E)-ethyl 4-(benzylideneamino)-3-(2-(N,4-dimethylphenylsulfonamido)-2-oxoethyl)benzoate

: C₂₆H₂₈N₂O₅S

Guidance literature:: With sodium cyanoborohydride; In tetrahydrofuran; at 28 ℃; for 0.333333h;
DOI:10.1021/ol302621z

Reference yield:

: 1403981-67-8
(E)-ethyl 4-(benzylideneamino)-3-(2-(N,4-dimethylphenylsulfonamido)-2-oxoethyl)benzoate

: 1403981-76-9
ethyl 1-benzyl-2-oxoindoline-5-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium cyanoborohydride / tetrahydrofuran / 0.33 h / 28 °C

2: siliaflash-G₆₀ / tetrahydrofuran / 1 h / 80 °C

With sodium cyanoborohydride; In tetrahydrofuran;
DOI:10.1021/ol302621z