[3-(4-Methylsulfanylcarbonimidoyl-phenyl)-2-(toluene-4-sulfonylamino)-propionylamino]-acetic acid; hydriodide

Base Information

Chemical Name:[3-(4-Methylsulfanylcarbonimidoyl-phenyl)-2-(toluene-4-sulfonylamino)-propionylamino]-acetic acid; hydriodide
CAS No.:90282-07-8
Molecular Formula:C₂₀H₂₃N₃O₅S₂*HI
Molecular Weight:577.464
Hs Code.:

Synonyms:[3-(4-Methylsulfanylcarbonimidoyl-phenyl)-2-(toluene-4-sulfonylamino)-propionylamino]-acetic acid; hydriodide

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Chemical Property of [3-(4-Methylsulfanylcarbonimidoyl-phenyl)-2-(toluene-4-sulfonylamino)-propionylamino]-acetic acid; hydriodide

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Technology Process of [3-(4-Methylsulfanylcarbonimidoyl-phenyl)-2-(toluene-4-sulfonylamino)-propionylamino]-acetic acid; hydriodide

There total 6 articles about [3-(4-Methylsulfanylcarbonimidoyl-phenyl)-2-(toluene-4-sulfonylamino)-propionylamino]-acetic acid; hydriodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 90282-06-7
[3-(4-Thiocarbamoyl-phenyl)-2-(toluene-4-sulfonylamino)-propionylamino]-acetic acid

: 74-88-4
methyl iodide

: 90282-07-8
[3-(4-Methylsulfanylcarbonimidoyl-phenyl)-2-(toluene-4-sulfonylamino)-propionylamino]-acetic acid; hydriodide

Guidance literature:: In acetone; for 16h; Ambient temperature;

Reference yield:

: 18910-26-4,22888-47-7
2-amino-3-(4-cyano-phenyl)-propionic acid

: 90282-07-8
[3-(4-Methylsulfanylcarbonimidoyl-phenyl)-2-(toluene-4-sulfonylamino)-propionylamino]-acetic acid; hydriodide

Guidance literature:: Multi-step reaction with 5 steps

1: KOH

2: 85 percent / SOCl₂ / 1 h / Heating

3: 68 percent / NaOH (1 mol/l) / benzene / 4 h / Ambient temperature

4: 65 percent / TEA, H₂S / pyridine / 36 h / Ambient temperature

5: 73 percent / acetone / 16 h / Ambient temperature

With potassium hydroxide; sodium hydroxide; thionyl chloride; TEA; hydrogen sulfide; In pyridine; acetone; benzene;

Reference yield:

: 80852-48-8
N-_α-Tosyl-4-cyanphenylalaninchlorid

: 90282-07-8
[3-(4-Methylsulfanylcarbonimidoyl-phenyl)-2-(toluene-4-sulfonylamino)-propionylamino]-acetic acid; hydriodide

Guidance literature:: Multi-step reaction with 3 steps

1: 68 percent / NaOH (1 mol/l) / benzene / 4 h / Ambient temperature

2: 65 percent / TEA, H₂S / pyridine / 36 h / Ambient temperature

3: 73 percent / acetone / 16 h / Ambient temperature

With sodium hydroxide; TEA; hydrogen sulfide; In pyridine; acetone; benzene;