N-[3-cyano-3-(phenylmethoxy)-1(3H)-isobenzofuranylidene]-2,4,4-trimethyl-2-pentanamine

Base Information

Chemical Name:N-[3-cyano-3-(phenylmethoxy)-1(3H)-isobenzofuranylidene]-2,4,4-trimethyl-2-pentanamine
CAS No.:1449007-84-4
Molecular Formula:C₂₄H₂₈N₂O₂
Molecular Weight:376.499
Hs Code.:

Synonyms:N-[3-cyano-3-(phenylmethoxy)-1(3H)-isobenzofuranylidene]-2,4,4-trimethyl-2-pentanamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[3-cyano-3-(phenylmethoxy)-1(3H)-isobenzofuranylidene]-2,4,4-trimethyl-2-pentanamine

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Technology Process of N-[3-cyano-3-(phenylmethoxy)-1(3H)-isobenzofuranylidene]-2,4,4-trimethyl-2-pentanamine

There total 2 articles about N-[3-cyano-3-(phenylmethoxy)-1(3H)-isobenzofuranylidene]-2,4,4-trimethyl-2-pentanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

: 5532-86-5
benzyl cyanoformate

: 14542-93-9
1,1,3,3-tetramethylbutane isonitrile

: 88284-48-4
2-(trimethylsilyl)phenyl trifluoromethanesulfonate

: 1449007-84-4
N-[3-cyano-3-(phenylmethoxy)-1(3H)-isobenzofuranylidene]-2,4,4-trimethyl-2-pentanamine

Guidance literature:: With potassium fluoride; palladium(II)[(1,1'-bis(diphenylphosphino)ferrocene)(C₆H₅CN)2]*2BF₄; 18-crown-6 ether; In tetrahydrofuran; at 50 ℃; for 18h; Schlenk technique; Inert atmosphere;
DOI:10.3987/COM-12-S(N)77

Reference yield: 51.0%

: 5532-86-5
benzyl cyanoformate

: 14542-93-9
1,1,3,3-tetramethylbutane isonitrile

: 88284-48-4
2-(trimethylsilyl)phenyl trifluoromethanesulfonate

: 1449007-84-4
N-[3-cyano-3-(phenylmethoxy)-1(3H)-isobenzofuranylidene]-2,4,4-trimethyl-2-pentanamine

: 1615677-46-7
(Z)-benzyl 2-[cyano(2,4,4-trimethylpentan-2-ylimino)methyl]benzoate

Guidance literature:: With potassium fluoride; [Pd(PhCN)₂(dppf)](BF₄)₂; 18-crown-6 ether; In tetrahydrofuran; at 50 ℃; for 18h; Schlenk technique; Inert atmosphere;
DOI:10.1021/om500408h

Reference yield: 82.0%

: 1449007-84-4
N-[3-cyano-3-(phenylmethoxy)-1(3H)-isobenzofuranylidene]-2,4,4-trimethyl-2-pentanamine

: 14542-93-9
1,1,3,3-tetramethylbutane isonitrile

: benzyl 2-cyanobenzoate

Guidance literature:: With tris(pentafluorophenyl)borate; In tetrahydrofuran; at 70 ℃; for 8h; Inert atmosphere; Schlenk technique;
DOI:10.1021/ol5026519