Benzenamine, N-(2-chloroethyl)-N-ethyl-4-[(4-nitrophenyl)azo]-

Base Information

Chemical Name:Benzenamine, N-(2-chloroethyl)-N-ethyl-4-[(4-nitrophenyl)azo]-
CAS No.:55619-06-2
Molecular Formula:C16H17 Cl N4 O2
Molecular Weight:332.79
Hs Code.:
European Community (EC) Number:259-724-2
UNII:4VF3BRY5YK
DSSTox Substance ID:DTXSID6069034
Nikkaji Number:J267.034H
Mol file:55619-06-2.mol

Synonyms:55619-06-2;EINECS 259-724-2;Benzenamine, N-(2-chloroethyl)-N-ethyl-4-[(4-nitrophenyl)azo]-;Benzenamine, N-(2-chloroethyl)-N-ethyl-4-((4-nitrophenyl)azo)-;N-(2-CHLOROETHYL)-N-ETHYL-4-[(4-NITROPHENYL)AZO]ANILINE;Aniline, N-(2-chloroethyl)-N-ethyl-4-((p-nitrophenyl)azo)-;Benzenamine, N-(2-chloroethyl)-N-ethyl-4-(2-(4-nitrophenyl)diazenyl)-;N-(2-Chloroethyl)-N-ethyl-4-((4-nitrophenyl)azo)aniline;Benzenamine, N-(2-chloroethyl)-N-ethyl-4-[2-(4-nitrophenyl)diazenyl]-;4VF3BRY5YK;DTXSID6069034;N-(2-Chloroethyl)-N-ethyl-4-[(4-nitrophenyl)azo]benzenamine;N-(2-Chloroethyl)-N-ethyl-4-[2-(4-nitrophenyl)diazenyl]benzenamine

Suppliers and Price of Benzenamine, N-(2-chloroethyl)-N-ethyl-4-[(4-nitrophenyl)azo]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of Benzenamine, N-(2-chloroethyl)-N-ethyl-4-[(4-nitrophenyl)azo]-

Chemical Property:

Vapor Pressure:1.22E-10mmHg at 25°C
Boiling Point:513.1°Cat760mmHg
Flash Point:264.1°C
PSA：73.78000
Density:1.24g/cm³
LogP:5.59850
XLogP3:4.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:6
Exact Mass:332.1040035
Heavy Atom Count:23
Complexity:386

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCN(CCCl)C1=CC=C(C=C1)N=NC2=CC=C(C=C2)[N+](=O)[O-]

Technology Process of Benzenamine, N-(2-chloroethyl)-N-ethyl-4-[(4-nitrophenyl)azo]-

There total 3 articles about Benzenamine, N-(2-chloroethyl)-N-ethyl-4-[(4-nitrophenyl)azo]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.9%

: 92-49-9
N-ethyl-N-(2-chloroethyl)aniline

: 456-27-9
4-nitrobenzenediazonium tetrafluoroborate

: 55619-06-2
N-(2-chloroethyl)-N-ethyl-4-[(4-nitrophenyl)azo]aniline

Guidance literature:: In N,N-dimethyl-formamide; at 0 ℃; for 24h;
DOI:10.1039/c5tc00182j

Reference yield:

: 103-69-5
N-ethyl-N-phenylamine

: 55619-06-2
N-(2-chloroethyl)-N-ethyl-4-[(4-nitrophenyl)azo]aniline

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 24 h / 80 °C

2: trichlorophosphate / 2 h / 110 °C

3: N,N-dimethyl-formamide / 24 h / 0 °C

With potassium carbonate; potassium iodide; trichlorophosphate; In N,N-dimethyl-formamide;
DOI:10.1039/c5tc00182j

Reference yield:

: 92-50-2
2-( N-ethylanilino)ethanol

: 55619-06-2
N-(2-chloroethyl)-N-ethyl-4-[(4-nitrophenyl)azo]aniline

Guidance literature:: Multi-step reaction with 2 steps

1: trichlorophosphate / 2 h / 110 °C

2: N,N-dimethyl-formamide / 24 h / 0 °C

With trichlorophosphate; In N,N-dimethyl-formamide;
DOI:10.1039/c5tc00182j