N'-<5-<<4-<<5-pentyl>amino>-1,4-dioxobutyl>(phenylmethoxy)amino>pentyl>-N-(4-(ethoxycarbonyl)butyl)-N-(phenylmethoxy)butanediamide

Base Information

• Chemical Name: N'-<5-<<4-<<5-pentyl>amino>-1,4-dioxobutyl>(phenylmethoxy)amino>pentyl>-N-(4-(ethoxycarbonyl)butyl)-N-(phenylmethoxy)butanediamide
• CAS No.: 123152-40-9
• Molecular Formula: C₄₈H₆₇N₅O₁₀
• Molecular Weight: 874.087

Synonyms:N'-<5-<<4-<<5-pentyl>amino>-1,4-dioxobutyl>(phenylmethoxy)amino>pentyl>-N-(4-(ethoxycarbonyl)butyl)-N-(phenylmethoxy)butanediamide

Chemical Property of N'-<5-<<4-<<5-pentyl>amino>-1,4-dioxobutyl>(phenylmethoxy)amino>pentyl>-N-(4-(ethoxycarbonyl)butyl)-N-(phenylmethoxy)butanediamide

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of N'-<5-<<4-<<5-pentyl>amino>-1,4-dioxobutyl>(phenylmethoxy)amino>pentyl>-N-(4-(ethoxycarbonyl)butyl)-N-(phenylmethoxy)butanediamide

There total 2 articles about N'-<5-<<4-<<5-pentyl>amino>-1,4-dioxobutyl>(phenylmethoxy)amino>pentyl>-N-(4-(ethoxycarbonyl)butyl)-N-(phenylmethoxy)butanediamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N'-<5-<<4-<<5-pentyl>amino>-1,4-dioxobutyl>(phenylmethoxy)amino>pentyl>-N-(5-ethoxy-5-iminopentyl)-N-(phenylmethoxy)butanediamide hydrochloride (123152-39-6) → N'-<5-<<4-<<5-pentyl>amino>-1,4-dioxobutyl>(phenylmethoxy)amino>pentyl>-N-(4-(ethoxycarbonyl)butyl)-N-(phenylmethoxy)butanediamide (123152-40-9)

Guidance literature:

With water; at 0 ℃; for 6h; Yield given;

DOI:10.1021/jo00284a044

Reference yield:

N'-<5-<<4-<<5-pentyl>amino>-1,4-dioxobutyl>(phenylmethoxy)amino>pentyl>-N-(4-cyanobutyl)-N-(phenylmethoxy)butanediamide (112139-65-8) → N'-<5-<<4-<<5-pentyl>amino>-1,4-dioxobutyl>(phenylmethoxy)amino>pentyl>-N-(4-(ethoxycarbonyl)butyl)-N-(phenylmethoxy)butanediamide (123152-40-9)

Guidance literature:

Multi-step reaction with 2 steps

1: HCl (gas) / 20 h / -20 °C

2: H₂O / 6 h / 0 °C

With hydrogenchloride; water;

DOI:10.1021/jo00284a044

Reference yield: 55.0%

N'-<5-<<4-<<5-pentyl>amino>-1,4-dioxobutyl>(phenylmethoxy)amino>pentyl>-N-(4-(ethoxycarbonyl)butyl)-N-(phenylmethoxy)butanediamide (123152-40-9) → N'-<5-<<4-<<5-pentyl>amino>-1,4-dioxobutyl>(phenylmethoxy)amino>pentyl>-N-(4-carboxybutyl)-N-(phenylmethoxy)butanediamide (123152-41-0)

Guidance literature:

With potassium hydroxide; In acetone; Ambient temperature;

DOI:10.1021/jo00284a044

upstream raw materials:

N'-<5-<<4-<<5-pentyl>amino>-1,4-dioxobutyl>(phenylmethoxy)amino>pentyl>-N-(5-ethoxy-5-iminopentyl)-N-(phenylmethoxy)butanediamide hydrochloride

N'-<5-<<4-<<5-pentyl>amino>-1,4-dioxobutyl>(phenylmethoxy)amino>pentyl>-N-(4-cyanobutyl)-N-(phenylmethoxy)butanediamide

Downstream raw materials:

N'-<5-<<4-<<5-pentyl>amino>-1,4-dioxobutyl>(phenylmethoxy)amino>pentyl>-N-(4-carboxybutyl)-N-(phenylmethoxy)butanediamide

N'-<5-<<4-<<5-pentyl>amino>-1,4-dioxobutyl>(phenylmethoxy)amino>pentyl>-N-(5-hydroxypentyl)-N-(phenylmethoxy)butanediamide

N'-<5-<<4-<<5-pentyl>amino>-1,4-dioxobutyl>(phenylmethoxy)amino>pentyl>-N-(4-((phenylthio)carbonyl)butyl)-N-(phenylmethoxy)butanediamide

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