Technology Process of C37H50O4
There total 19 articles about C37H50O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
In
tetrahydrofuran;
at 20 ℃;
for 0.5h;
Inert atmosphere;
DOI:10.1021/ol1019663
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere
2.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 0 - 20 °C / Inert atmosphere
3.1: lithium aluminium tetrahydride / tetrahydrofuran / -10 °C / Inert atmosphere; Reflux
4.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 0 - 20 °C / Inert atmosphere
4.2: 0 °C / Inert atmosphere; Reflux
5.1: pyridine hydrochloride / 2 h / 135 °C / Inert atmosphere
6.1: chromium(VI) oxide; sodium acetate; acetic anhydride; acetic acid / water / 0.67 h / 0 °C / Inert atmosphere
7.1: tetrahydrofuran / 20 °C / Inert atmosphere
With
chromium(VI) oxide; lithium aluminium tetrahydride; di-isopropyl azodicarboxylate; tetrabutyl ammonium fluoride; sodium acetate; pyridine hydrochloride; acetic anhydride; sodium hydride; acetic acid; triphenylphosphine;
In
tetrahydrofuran; water; mineral oil;
2.1: Mitsunobu reaction / 5.1: Marker's degradation / 7.1: Grignard reaction;
DOI:10.1021/jo102054r
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: lithium aluminium tetrahydride / tetrahydrofuran / -10 °C / Inert atmosphere; Reflux
2.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 0 - 20 °C / Inert atmosphere
2.2: 0 °C / Inert atmosphere; Reflux
3.1: pyridine hydrochloride / 2 h / 135 °C / Inert atmosphere
4.1: chromium(VI) oxide; sodium acetate; acetic anhydride; acetic acid / water / 0.67 h / 0 °C / Inert atmosphere
5.1: tetrahydrofuran / 20 °C / Inert atmosphere
With
chromium(VI) oxide; lithium aluminium tetrahydride; sodium acetate; pyridine hydrochloride; acetic anhydride; sodium hydride; acetic acid;
In
tetrahydrofuran; water; mineral oil;
3.1: Marker's degradation / 5.1: Grignard reaction;
DOI:10.1021/jo102054r