Technology Process of Clorindione
There total 12 articles about Clorindione which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
1,4-diaza-bicyclo[2.2.2]octane; bis(di-tert-?butyl(4-?dimethylaminophenyl)?phosphine)?dichloropalladium(II); trimethylphosphine(hexafluoroacetylacetonato)copper(I); 1-butyl-3-methylimidazolium trifluoromethanesulfonimide salt; silver trifluoromethanesulfonate;
In
ethylene glycol; dimethyl sulfoxide;
at 90 ℃;
for 2h;
Reagent/catalyst;
Inert atmosphere;
- Guidance literature:
-
With
dichloro bis(acetonitrile) palladium(II); potassium tert-butylate; tert-butyl XPhos;
In
1,4-dioxane;
at 110 ℃;
for 12h;
Sealed tube;
Inert atmosphere;
DOI:10.1021/acs.joc.1c01149
- Guidance literature:
-
With
sodium ethanolate;
In
ethanol;
for 1.5h;
Heating;
DOI:10.1021/jm00149a008