N₆-((8-methyl-2-o-tolylquinolin-3-yl)methyl)-9H-purine-2,6-diamine

Base Information

Chemical Name:N₆-((8-methyl-2-o-tolylquinolin-3-yl)methyl)-9H-purine-2,6-diamine
CAS No.:1065478-40-1
Molecular Formula:C₂₃H₂₁N₇
Molecular Weight:395.467
Hs Code.:

N<sub>6</sub>-((8-methyl-2-o-tolylquinolin-3-yl)methyl)-9H-purine-2,6-diamine

Synonyms:N₆-((8-methyl-2-o-tolylquinolin-3-yl)methyl)-9H-purine-2,6-diamine

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Chemical Property of N₆-((8-methyl-2-o-tolylquinolin-3-yl)methyl)-9H-purine-2,6-diamine

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Technology Process of N₆-((8-methyl-2-o-tolylquinolin-3-yl)methyl)-9H-purine-2,6-diamine

There total 7 articles about N₆-((8-methyl-2-o-tolylquinolin-3-yl)methyl)-9H-purine-2,6-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 73568-26-0
2-chloro-8-methyl-quinoline-3-carbaldehyde

: 1065478-40-1
N₆-((8-methyl-2-o-tolylquinolin-3-yl)methyl)-9H-purine-2,6-diamine

Guidance literature:: Multi-step reaction with 6 steps

1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; acetonitrile / 100 °C

2: sodium tetrahydroborate / tetrahydrofuran / 2 h / 0 °C

3: thionyl chloride / chloroform / 2 h / 20 °C

4: sodium azide / dimethyl sulfoxide / 4 h / 20 °C

5: hydrogen / palladium 10% on activated carbon / methanol / 8 h / 20 °C

6: triethylamine / isopropyl alcohol / 1.33 h / 150 °C / Microwave irradiation

With sodium tetrahydroborate; thionyl chloride; sodium azide; hydrogen; sodium carbonate; triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium 10% on activated carbon; In tetrahydrofuran; methanol; chloroform; water; dimethyl sulfoxide; isopropyl alcohol; acetonitrile;

Reference yield:

: 1065483-04-6
(8-methyl-2-o-tolylquinolin-3-yl)methanamine

: 10310-21-1
2-amino-6-chloropurine

: 1065478-40-1
N₆-((8-methyl-2-o-tolylquinolin-3-yl)methyl)-9H-purine-2,6-diamine

Guidance literature:: With triethylamine; In isopropyl alcohol; at 150 ℃; for 1.33333h; Microwave irradiation;

Reference yield:

: 1065480-84-3
8-methyl-2-o-tolylquinoline-3-carbaldehyde

: 1065478-40-1
N₆-((8-methyl-2-o-tolylquinolin-3-yl)methyl)-9H-purine-2,6-diamine

Guidance literature:: Multi-step reaction with 5 steps

1: sodium tetrahydroborate / tetrahydrofuran / 2 h / 0 °C

2: thionyl chloride / chloroform / 2 h / 20 °C

3: sodium azide / dimethyl sulfoxide / 4 h / 20 °C

4: hydrogen / palladium 10% on activated carbon / methanol / 8 h / 20 °C

5: triethylamine / isopropyl alcohol / 1.33 h / 150 °C / Microwave irradiation

With sodium tetrahydroborate; thionyl chloride; sodium azide; hydrogen; triethylamine; palladium 10% on activated carbon; In tetrahydrofuran; methanol; chloroform; dimethyl sulfoxide; isopropyl alcohol;